t-butyl (S,E)-12-(2-(benzyloxycarbonylamino)-3-phenylpropanoyloxy)dodec-2-enoate

Base Information

Chemical Name:t-butyl (S,E)-12-(2-(benzyloxycarbonylamino)-3-phenylpropanoyloxy)dodec-2-enoate
CAS No.:1019646-11-7
Molecular Formula:C₃₃H₄₅NO₆
Molecular Weight:551.723
Hs Code.:

Synonyms:t-butyl (S,E)-12-(2-(benzyloxycarbonylamino)-3-phenylpropanoyloxy)dodec-2-enoate

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Chemical Property of t-butyl (S,E)-12-(2-(benzyloxycarbonylamino)-3-phenylpropanoyloxy)dodec-2-enoate

Chemical Property:

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Technology Process of t-butyl (S,E)-12-(2-(benzyloxycarbonylamino)-3-phenylpropanoyloxy)dodec-2-enoate

There total 3 articles about t-butyl (S,E)-12-(2-(benzyloxycarbonylamino)-3-phenylpropanoyloxy)dodec-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 1309476-87-6
(S)-11-methyldodec-10-en-1-yl 2-(benzyloxycarbonylamino)-3-phenylpropanoate

: 1019646-11-7
t-butyl (S,E)-12-(2-(benzyloxycarbonylamino)-3-phenylpropanoyloxy)dodec-2-enoate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; toluene-4-sulfonic acid; In water; at 22 ℃; for 12h; Sealed vial; Inert atmosphere;
DOI:10.1021/jo200746y

Reference yield: 96.0%

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 1019646-00-4
N-carbobenzyloxy-L-phenylalanine 10-undecenyl ester

: 1019646-11-7
t-butyl (S,E)-12-(2-(benzyloxycarbonylamino)-3-phenylpropanoyloxy)dodec-2-enoate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In water; at 22 ℃; for 12h; stereoselective reaction; Micellar solution;
DOI:10.1021/ol800028x

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 11-methyldodec-10-en-1-ol

: 1019646-11-7
t-butyl (S,E)-12-(2-(benzyloxycarbonylamino)-3-phenylpropanoyloxy)dodec-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 h / 0 - 20 °C / Inert atmosphere

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; toluene-4-sulfonic acid / water / 12 h / 22 °C / Sealed vial; Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water;
DOI:10.1021/jo200746y