2,2'-Bis<2-<2-<2-<<(4-methylphenyl)sulfonyl>oxy>ethoxy>ethoxy>ethoxy>-N-<5-methyl-2-(2-propenyloxy)phenyl>-<1,1'-binaphthalene>-3-carboxamide

Base Information

Chemical Name:2,2'-Bis<2-<2-<2-<<(4-methylphenyl)sulfonyl>oxy>ethoxy>ethoxy>ethoxy>-N-<5-methyl-2-(2-propenyloxy)phenyl>-<1,1'-binaphthalene>-3-carboxamide
CAS No.:155580-18-0
Molecular Formula:C₅₇H₆₁NO₁₄S₂
Molecular Weight:1048.24
Hs Code.:

Synonyms:2,2'-Bis<2-<2-<2-<<(4-methylphenyl)sulfonyl>oxy>ethoxy>ethoxy>ethoxy>-N-<5-methyl-2-(2-propenyloxy)phenyl>-<1,1'-binaphthalene>-3-carboxamide

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Chemical Property of 2,2'-Bis<2-<2-<2-<<(4-methylphenyl)sulfonyl>oxy>ethoxy>ethoxy>ethoxy>-N-<5-methyl-2-(2-propenyloxy)phenyl>-<1,1'-binaphthalene>-3-carboxamide

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Technology Process of 2,2'-Bis<2-<2-<2-<<(4-methylphenyl)sulfonyl>oxy>ethoxy>ethoxy>ethoxy>-N-<5-methyl-2-(2-propenyloxy)phenyl>-<1,1'-binaphthalene>-3-carboxamide

There total 8 articles about 2,2'-Bis<2-<2-<2-<<(4-methylphenyl)sulfonyl>oxy>ethoxy>ethoxy>ethoxy>-N-<5-methyl-2-(2-propenyloxy)phenyl>-<1,1'-binaphthalene>-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 98-59-9
p-toluenesulfonyl chloride

: 155580-16-8
2,2'-Bis<2-<2-(2-hydroxyethoxy)ethoxy>ethoxy>-N-<5-methyl-2-(2-propenyloxy)phenyl>-<1,1'-binaphthalene>-3-carboxamide

: 155580-18-0
2,2'-Bis<2-<2-<2-<<(4-methylphenyl)sulfonyl>oxy>ethoxy>ethoxy>ethoxy>-N-<5-methyl-2-(2-propenyloxy)phenyl>-<1,1'-binaphthalene>-3-carboxamide

Guidance literature:: With pyridine; at 0 ℃; for 3h;
DOI:10.1002/recl.19931121106

Reference yield:

: 55489-58-2,1201808-31-2
triethylene glycol monobenzyl ether

: 155580-18-0
2,2'-Bis<2-<2-<2-<<(4-methylphenyl)sulfonyl>oxy>ethoxy>ethoxy>ethoxy>-N-<5-methyl-2-(2-propenyloxy)phenyl>-<1,1'-binaphthalene>-3-carboxamide

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine

2: 85 percent / K₂CO₃ / acetonitrile / Heating

3: 100 percent / aq. KOH / methanol / 1 h / Heating

4: 1.) HOBT*H₂O, DCC / 1.) CH₂Cl₂, r.t., 1 h, 2.) overnight

5: 100 percent / H₂ / 10percent Pd-C / ethyl acetate; ethanol

6: 100 percent / K₂CO₃ / acetonitrile / 3 h / Heating

7: 85 percent / pyridine / 3 h / 0 °C

With pyridine; potassium hydroxide; hydrogen; potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; ethyl acetate; acetonitrile;
DOI:10.1002/recl.19931121106

Reference yield:

: 84131-04-4
triethylene glycol monobenzyl tosyl ether

: 155580-18-0
2,2'-Bis<2-<2-<2-<<(4-methylphenyl)sulfonyl>oxy>ethoxy>ethoxy>ethoxy>-N-<5-methyl-2-(2-propenyloxy)phenyl>-<1,1'-binaphthalene>-3-carboxamide

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / K₂CO₃ / acetonitrile / Heating

2: 100 percent / aq. KOH / methanol / 1 h / Heating

3: 1.) HOBT*H₂O, DCC / 1.) CH₂Cl₂, r.t., 1 h, 2.) overnight

4: 100 percent / H₂ / 10percent Pd-C / ethyl acetate; ethanol

5: 100 percent / K₂CO₃ / acetonitrile / 3 h / Heating

6: 85 percent / pyridine / 3 h / 0 °C

With pyridine; potassium hydroxide; hydrogen; potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; ethyl acetate; acetonitrile;
DOI:10.1002/recl.19931121106