C₂₆H₂₃ClO₇

Base Information

Chemical Name:C₂₆H₂₃ClO₇
CAS No.:1402931-91-2
Molecular Formula:C₂₆H₂₃ClO₇
Molecular Weight:482.917
Hs Code.:

C<sub>26</sub>H<sub>23</sub>ClO<sub>7</sub>

Synonyms:C₂₆H₂₃ClO₇

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Chemical Property of C₂₆H₂₃ClO₇

Chemical Property:

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Technology Process of C₂₆H₂₃ClO₇

There total 16 articles about C₂₆H₂₃ClO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 960365-65-5
(1R,2R,3S,3aR,8bS)-methyl 1,6,8b-trihydroxy-8-methoxy-3a-(4-methoxyphenyl)-3-phenyl-2,3,3a,8b-tetrahydro-1H-benzo[b]-cyclopenta[d]furan-2-carboxylate

: 1402931-91-2
C₂₆H₂₃ClO₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.82 h / -10 °C / Inert atmosphere

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine / 1,4-dioxane / 14 h / Inert atmosphere; Reflux

3.1: copper dichloride / methanol / 3 h / Inert atmosphere; Reflux

4.1: lithium hydroxide / methanol; water / 16 h / 45 °C / Inert atmosphere

4.2: Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine; N-ethyl-N,N-diisopropylamine; copper dichloride; lithium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water;
DOI:10.1021/jm3011542

Reference yield:

: 1402931-76-3
(1R,2R,3S,3aR,8bS)-methyl 6-chloro-1,8b-dihydroxy-8-methoxy-3a-(4-methoxyphenyl)-3-phenyl-2,3,3a,8b-tetrahydro-1H-benzo[b]-cyclopenta[d]furan-2-carboxylate

: 1402931-91-2
C₂₆H₂₃ClO₇

Guidance literature:: (1R,2R,3S,3aR,8bS)-methyl 6-chloro-1,8b-dihydroxy-8-methoxy-3a-(4-methoxyphenyl)-3-phenyl-2,3,3a,8b-tetrahydro-1H-benzo[b]-cyclopenta[d]furan-2-carboxylate; With lithium hydroxide; In methanol; water; at 45 ℃; for 16h; Inert atmosphere;

With hydrogenchloride; In methanol; water; Inert atmosphere;
DOI:10.1021/jm3011542

Reference yield:

: [2-[4-benzyloxy-2-methoxy-6-(4-methoxybenzoyl)oxyphenyl]-2-oxoethyl] 4-methoxybenzoate

: 1402931-91-2
C₂₆H₂₃ClO₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -70 - -20 °C / Inert atmosphere

2.1: sulfuric acid; acetic acid / 20 h / 20 °C / Inert atmosphere

3.1: water; sodium hydroxide / ethanol / 1 h / 80 °C / Inert atmosphere

4.1: methanol; dichloromethane; acetonitrile / 10 h / 0 - 5 °C / Inert atmosphere; UV-irradiation

4.2: 1 h / 60 °C / Inert atmosphere

4.3: 48 h / Inert atmosphere

5.1: 5%-palladium/activated carbon; hydrogen / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

6.1: ChiralPak AD-H / ethanol / Inert atmosphere; Supercritical conditions; Resolution of racemate

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.82 h / -10 °C / Inert atmosphere

8.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine / 1,4-dioxane / 14 h / Inert atmosphere; Reflux

9.1: copper dichloride / methanol / 3 h / Inert atmosphere; Reflux

10.1: lithium hydroxide / methanol; water / 16 h / 45 °C / Inert atmosphere

10.2: Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; 5%-palladium/activated carbon; water; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; copper dichloride; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; acetonitrile; 1.1: |Baker-Venkataraman Rearrangement;
DOI:10.1021/jm3011542