methyl 2-(3-(3-aminopropoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

Base Information

Chemical Name:methyl 2-(3-(3-aminopropoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate
CAS No.:1579977-64-2
Molecular Formula:C₂₇H₂₅NO₅
Molecular Weight:443.499
Hs Code.:

Synonyms:methyl 2-(3-(3-aminopropoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

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Chemical Property of methyl 2-(3-(3-aminopropoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

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Technology Process of methyl 2-(3-(3-aminopropoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

There total 5 articles about methyl 2-(3-(3-aminopropoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1579977-60-8
methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

: 1579977-64-2
methyl 2-(3-(3-aminopropoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

Guidance literature:: methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate; With zinc(II) chloride; In dichloromethane; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In dichloromethane;
DOI:10.1039/c3ob42326c

Reference yield:

: 1579977-56-2
C₂₄H₁₈O₅

: 1579977-64-2
methyl 2-(3-(3-aminopropoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 20 °C

2: zinc(II) chloride / dichloromethane / 3 h / 20 °C

With potassium carbonate; zinc(II) chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42326c

Reference yield:

: 518-45-6
fluorescein free acid

: 1579977-64-2
methyl 2-(3-(3-aminopropoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / 12 h / 85 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

3: sodium tetrahydroborate / methanol / 2.5 h / 0 - 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 6 h / 20 °C

5: zinc(II) chloride / dichloromethane / 3 h / 20 °C

With sodium tetrahydroborate; sulfuric acid; potassium carbonate; zinc(II) chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42326c