methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

Base Information

Chemical Name:methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate
CAS No.:1579977-60-8
Molecular Formula:C₃₂H₃₃NO₇
Molecular Weight:543.617
Hs Code.:

Synonyms:methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

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Chemical Property of methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

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Technology Process of methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

There total 4 articles about methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1579977-56-2
C₂₄H₁₈O₅

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 1579977-60-8
methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h;
DOI:10.1039/c3ob42326c

Reference yield:

: 70672-06-9
methyl 2-(6-hydroxy-3-oxo-3H-xanthen-9-yl)benzoate

: 1579977-60-8
methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

2: sodium tetrahydroborate / methanol / 2.5 h / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 6 h / 20 °C

With sodium tetrahydroborate; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42326c

Reference yield:

: 518-45-6
fluorescein free acid

: 1579977-60-8
methyl 2-(3-(3-((tert-butoxycarbonyl)amino)propoxy)-6-(prop-2-yn-1-yloxy)-9H-xanthen-9-yl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 12 h / 85 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

3: sodium tetrahydroborate / methanol / 2.5 h / 0 - 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 6 h / 20 °C

With sodium tetrahydroborate; sulfuric acid; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42326c