C₃₈H₄₂O₆

Base Information

Chemical Name:C₃₈H₄₂O₆
CAS No.:1320210-74-9
Molecular Formula:C₃₈H₄₂O₆
Molecular Weight:594.748
Hs Code.:

C<sub>38</sub>H<sub>42</sub>O<sub>6</sub>

Synonyms:C₃₈H₄₂O₆

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Chemical Property of C₃₈H₄₂O₆

Chemical Property:

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Technology Process of C₃₈H₄₂O₆

There total 8 articles about C₃₈H₄₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1320210-73-8
C₂₄H₃₀O₆

: 100-39-0
benzyl bromide

: 1320210-74-9
C₃₈H₄₂O₆

Guidance literature:: C₂₄H₃₀O₆; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; Inert atmosphere;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 60 ℃; for 19h; Inert atmosphere;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: 1320210-69-2
C₂₂H₂₄O₅

: 1320210-74-9
C₃₈H₄₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: benzene / 2 h / Inert atmosphere; Reflux

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

3.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

3.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

4.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

4.2: Saturated solution

5.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0 °C / Inert atmosphere

5.2: 19 h / 0 - 60 °C / Inert atmosphere

With titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; sodium hydride; diisobutylaluminium hydride; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; benzene; 1.1: Wittig reaction / 3.1: Sharpless epoxidation / 3.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: 100-39-0
benzyl bromide

: 1320210-74-9
C₃₈H₄₂O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere

2.1: ozone / methanol; dichloromethane / -78 °C

2.2: -78 - 20 °C

3.1: benzene / 2 h / Inert atmosphere; Reflux

4.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

5.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

5.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

6.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

6.2: Saturated solution

7.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0 °C / Inert atmosphere

7.2: 19 h / 0 - 60 °C / Inert atmosphere

With titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; sodium hydride; diisobutylaluminium hydride; ozone; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; benzene; 3.1: Wittig reaction / 5.1: Sharpless epoxidation / 5.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071