11-chloro-6-(4-methoxybenzyl)-pyrido[2',1':2,3]imidazo[5,4-c]benzazepin-7(6H)-one

Base Information

Chemical Name:11-chloro-6-(4-methoxybenzyl)-pyrido[2',1':2,3]imidazo[5,4-c]benzazepin-7(6H)-one
CAS No.:1220397-73-8
Molecular Formula:C₂₃H₁₈ClN₃O₂
Molecular Weight:403.868
Hs Code.:

Synonyms:11-chloro-6-(4-methoxybenzyl)-pyrido[2',1':2,3]imidazo[5,4-c]benzazepin-7(6H)-one

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Chemical Property of 11-chloro-6-(4-methoxybenzyl)-pyrido[2',1':2,3]imidazo[5,4-c]benzazepin-7(6H)-one

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Technology Process of 11-chloro-6-(4-methoxybenzyl)-pyrido[2',1':2,3]imidazo[5,4-c]benzazepin-7(6H)-one

There total 2 articles about 11-chloro-6-(4-methoxybenzyl)-pyrido[2',1':2,3]imidazo[5,4-c]benzazepin-7(6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1220397-47-6
N-(2-bromobenzyl)-6-chloro-N-(4-methoxybenzyl)-imidazo[1,2-a]pyridine-2-carboxamide

: 1220397-73-8
11-chloro-6-(4-methoxybenzyl)-pyrido[2',1':2,3]imidazo[5,4-c]benzazepin-7(6H)-one

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In ISOPROPYLAMIDE; at 130 ℃; for 2h; Microwave irradiation; Inert atmosphere;
DOI:10.1016/j.tet.2009.12.049

Reference yield: 51.0%

: 1220397-47-6
N-(2-bromobenzyl)-6-chloro-N-(4-methoxybenzyl)-imidazo[1,2-a]pyridine-2-carboxamide

: 1220397-67-0
6-(4-methoxybenzyl)-pyrido[2',1':2,3]imidazo[5,4-c]benzazepin-7(6H)-one

: 1220397-73-8
11-chloro-6-(4-methoxybenzyl)-pyrido[2',1':2,3]imidazo[5,4-c]benzazepin-7(6H)-one

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In ISOPROPYLAMIDE; at 130 ℃; for 2h; Microwave irradiation; Inert atmosphere;
DOI:10.1016/j.tet.2009.12.049

Reference yield: 85.0%

: 1220397-73-8
11-chloro-6-(4-methoxybenzyl)-pyrido[2',1':2,3]imidazo[5,4-c]benzazepin-7(6H)-one

: 87199-17-5
4-formylphenylboronic acid,

: C₃₀H₂₅N₃O₃

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; ethanol; at 150 ℃; for 2h; Microwave irradiation; Inert atmosphere;
DOI:10.1016/j.tet.2009.12.049