NC₅H₄CH₂NHC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2

Base Information

• Chemical Name: NC₅H₄CH₂NHC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2
• CAS No.: 1228351-42-5
• Molecular Formula: C₂₃H₃₁N₃
• Molecular Weight: 349.519
• Mol file: 1228351-42-5.mol

Synonyms:NC₅H₄CH₂NHC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2

Chemical Property of NC₅H₄CH₂NHC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of NC₅H₄CH₂NHC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2

There total 3 articles about NC₅H₄CH₂NHC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-(Aminomethyl)pyridine (3731-51-9) + 4-((2,6-di(isopropyl)phenyl)amino)-pent-3-en-2-one (205993-26-6) → NC5H4CH2NHC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2 (1228351-42-5)

Guidance literature:

In toluene; for 48h; Molecular sieve; Reflux;

DOI:10.1002/ejic.201701383

Reference yield:

2,6-diisopropylbenzenamine (24544-04-5) → NC5H4CH2NHC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2 (1228351-42-5)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / Inert atmosphere

2: toluene-4-sulfonic acid / toluene / 18 h / Reflux; Inert atmosphere; Dean-Stark

With toluene-4-sulfonic acid; In toluene;

DOI:10.1039/c6ra07453g

Reference yield:

acetylacetone (123-54-6,81235-32-7) → NC5H4CH2NHC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2 (1228351-42-5)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / Inert atmosphere

2: toluene-4-sulfonic acid / toluene / 18 h / Reflux; Inert atmosphere; Dean-Stark

With toluene-4-sulfonic acid; In toluene;

DOI:10.1039/c6ra07453g

upstream raw materials:

2-(Aminomethyl)pyridine

4-((2,6-di(isopropyl)phenyl)amino)-pent-3-en-2-one

2,6-diisopropylbenzenamine

acetylacetone

Downstream raw materials:

(NC₅H₄CH₂NC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2)Y(CH₂Si(CH₃)3)2

(NC₅H₄CH₂NC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2)Y(N(Si(CH₃)3)2)2

(NC₅H₄CH₂NC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2)La(N(Si(CH₃)3)2)2