5,7-dimethyl-6-oxo-3-aza-1-benzoylmethylazoniaadamantane bromide

Base Information

• Chemical Name: 5,7-dimethyl-6-oxo-3-aza-1-benzoylmethylazoniaadamantane bromide
• CAS No.: 137811-83-7
• Molecular Formula: Br*C₁₈H₂₃N₂O₂
• Molecular Weight: 379.297
• Mol file: 137811-83-7.mol

Synonyms:5,7-dimethyl-6-oxo-3-aza-1-benzoylmethylazoniaadamantane bromide

Chemical Property of 5,7-dimethyl-6-oxo-3-aza-1-benzoylmethylazoniaadamantane bromide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 5,7-dimethyl-6-oxo-3-aza-1-benzoylmethylazoniaadamantane bromide

There total 1 articles about 5,7-dimethyl-6-oxo-3-aza-1-benzoylmethylazoniaadamantane bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.3%

5,7-Dimethyl-6-oxo-1,3-diazaadamantane (80808-86-2) + α-bromoacetophenone (70-11-1) → 5,7-dimethyl-6-oxo-3-aza-1-benzoylmethylazoniaadamantane bromide (137811-83-7)

Guidance literature:

In benzene; at 20 ℃; for 2h;

DOI:10.1007/BF00474002

Reference yield: 65.6%

5,7-dimethyl-6-oxo-3-aza-1-benzoylmethylazoniaadamantane bromide (137811-83-7) → 2-benzoyl-6,8-dimethyl-7-oxo-1,4-diazatricyclo<4.3.1.14.8>undecane (137811-84-8)

Guidance literature:

With triethylamine; In water; at 80 ℃; for 3h;

DOI:10.1007/BF00474002

upstream raw materials:

5,7-Dimethyl-6-oxo-1,3-diazaadamantane

α-bromoacetophenone

Downstream raw materials:

2-benzoyl-6,8-dimethyl-7-oxo-1,4-diazatricyclo<4.3.1.1^4.8>undecane