11-hexyl-1-tosyl-2,3,4,5,6,11-hexahydro-1H-naphtho[2,3-b]azepane

Base Information

Chemical Name:11-hexyl-1-tosyl-2,3,4,5,6,11-hexahydro-1H-naphtho[2,3-b]azepane
CAS No.:1443365-88-5
Molecular Formula:C₂₇H₃₅NO₂S
Molecular Weight:437.646
Hs Code.:

Synonyms:11-hexyl-1-tosyl-2,3,4,5,6,11-hexahydro-1H-naphtho[2,3-b]azepane

Suppliers and Price of 11-hexyl-1-tosyl-2,3,4,5,6,11-hexahydro-1H-naphtho[2,3-b]azepane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-hexyl-1-tosyl-2,3,4,5,6,11-hexahydro-1H-naphtho[2,3-b]azepane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 11-hexyl-1-tosyl-2,3,4,5,6,11-hexahydro-1H-naphtho[2,3-b]azepane

There total 4 articles about 11-hexyl-1-tosyl-2,3,4,5,6,11-hexahydro-1H-naphtho[2,3-b]azepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 4233-33-4
4-Phenyl-1,2,4-triazolidine-3,5-dione

: 1443365-65-8
(Z)-2-heptylidene-3-methylene-1-tosylazepane

: 1443365-88-5
11-hexyl-1-tosyl-2,3,4,5,6,11-hexahydro-1H-naphtho[2,3-b]azepane

Guidance literature:: With cesium fluoride; In toluene; acetonitrile; at 60 ℃; for 16h; Inert atmosphere; Glovebox;
DOI:10.1002/adsc.201200703

Reference yield:

: 145782-21-4
N-(hex-5-yn-1-yl)-4-methylbenzenesulfonamide

: 1443365-88-5
11-hexyl-1-tosyl-2,3,4,5,6,11-hexahydro-1H-naphtho[2,3-b]azepane

Guidance literature:: Multi-step reaction with 4 steps

1: boron tribromide / dichloromethane

2: 1,10-Phenanthroline; potassium phosphate; copper(ll) sulfate pentahydrate / toluene / 16 h / 70 °C

3: potassium carbonate / ethanol / 1.75 h / 80 °C

4: cesium fluoride / toluene; acetonitrile / 16 h / 60 °C / Inert atmosphere; Glovebox

With potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; boron tribromide; potassium carbonate; cesium fluoride; In ethanol; dichloromethane; toluene; acetonitrile; 4: |Diels-Alder Cycloaddition;
DOI:10.1002/adsc.201200703

Reference yield:

: 18303-04-3
N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

: 1443365-88-5
11-hexyl-1-tosyl-2,3,4,5,6,11-hexahydro-1H-naphtho[2,3-b]azepane

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: boron tribromide / dichloromethane

3: 1,10-Phenanthroline; potassium phosphate; copper(ll) sulfate pentahydrate / toluene / 16 h / 70 °C

4: potassium carbonate / ethanol / 1.75 h / 80 °C

5: cesium fluoride / toluene; acetonitrile / 16 h / 60 °C / Inert atmosphere; Glovebox

With potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; di-isopropyl azodicarboxylate; boron tribromide; potassium carbonate; triphenylphosphine; cesium fluoride; In tetrahydrofuran; ethanol; dichloromethane; toluene; acetonitrile; 5: |Diels-Alder Cycloaddition;
DOI:10.1002/adsc.201200703