cis-3,5-O-benzylidenecyclohexanol

Base Information

Chemical Name:cis-3,5-O-benzylidenecyclohexanol
CAS No.:310904-10-0
Molecular Formula:C₁₃H₁₆O₃
Molecular Weight:220.268
Hs Code.:

Synonyms:cis-3,5-O-benzylidenecyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-3,5-O-benzylidenecyclohexanol

Chemical Property:

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Technology Process of cis-3,5-O-benzylidenecyclohexanol

There total 3 articles about cis-3,5-O-benzylidenecyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 74091-54-6
3-Phenyl-2,4,10-trioxa-adamantane

: 310904-10-0
cis-3,5-O-benzylidenecyclohexanol

Guidance literature:: With borane-THF; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -15 ℃; for 60h;
DOI:10.1248/cpb.48.1545

Reference yield:

: 50409-12-6,13314-30-2
cis,cis-1,3,5-trihydroxycyclohexane

: 310904-10-0
cis-3,5-O-benzylidenecyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / BF₃*Et₂O / CH₂Cl₂ / 20 °C

2: 70 percent / BH₃*THF / tetrahydrofuran; hexamethylphosphoric acid triamide / 60 h / -15 °C

With borane-THF; boron trifluoride diethyl etherate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1248/cpb.48.1545

Reference yield:

: 707-07-3
orthobenzoic acid trimethyl ester

: 310904-10-0
cis-3,5-O-benzylidenecyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / BF₃*Et₂O / CH₂Cl₂ / 20 °C

2: 70 percent / BH₃*THF / tetrahydrofuran; hexamethylphosphoric acid triamide / 60 h / -15 °C

With borane-THF; boron trifluoride diethyl etherate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1248/cpb.48.1545