N-(trifluoroacetyl)-1-<2,5-dimethoxy-4-(3-phenylpropyl)phenyl>-2-aminopropane

Base Information

Chemical Name:N-(trifluoroacetyl)-1-<2,5-dimethoxy-4-(3-phenylpropyl)phenyl>-2-aminopropane
CAS No.:125903-65-3
Molecular Formula:C₂₂H₂₆F₃NO₃
Molecular Weight:409.449
Hs Code.:

Synonyms:N-(trifluoroacetyl)-1-<2,5-dimethoxy-4-(3-phenylpropyl)phenyl>-2-aminopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(trifluoroacetyl)-1-<2,5-dimethoxy-4-(3-phenylpropyl)phenyl>-2-aminopropane

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Technology Process of N-(trifluoroacetyl)-1-<2,5-dimethoxy-4-(3-phenylpropyl)phenyl>-2-aminopropane

There total 3 articles about N-(trifluoroacetyl)-1-<2,5-dimethoxy-4-(3-phenylpropyl)phenyl>-2-aminopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 125926-55-8
N-(trifluoroacetyl)-1-(2,5-dimethoxy-4-hydrocinnamoylphenyl)-2-aminopropane

: 125903-65-3
N-(trifluoroacetyl)-1-<2,5-dimethoxy-4-(3-phenylpropyl)phenyl>-2-aminopropane

Guidance literature:: With perchloric acid; hydrogen; palladium on activated charcoal; In acetic acid; for 6h;
DOI:10.1021/jm00165a023

Reference yield:

: 2801-68-5
2,5-dimethoxyphenylisopropylamine

: 125903-65-3
N-(trifluoroacetyl)-1-<2,5-dimethoxy-4-(3-phenylpropyl)phenyl>-2-aminopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / 2 h / Ambient temperature

2: 44 percent / titanium tetrachloride / CH₂Cl₂ / 1.) -30 deg C, 30 min, 2.) RT, 3 d

3: 63 percent / H₂, 60percent aq. HClO₄ / 10percent Pd/C / acetic acid / 6 h

With perchloric acid; hydrogen; titanium tetrachloride; palladium on activated charcoal; In dichloromethane; acetic acid;
DOI:10.1021/jm00165a023

Reference yield:

: 79315-43-8
(+/-)-N-[2-(2,5-dimethoxyphenyl)-1-methylethyl]-2,2,2-trifluoroacetamide

: 125903-65-3
N-(trifluoroacetyl)-1-<2,5-dimethoxy-4-(3-phenylpropyl)phenyl>-2-aminopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / titanium tetrachloride / CH₂Cl₂ / 1.) -30 deg C, 30 min, 2.) RT, 3 d

2: 63 percent / H₂, 60percent aq. HClO₄ / 10percent Pd/C / acetic acid / 6 h

With perchloric acid; hydrogen; titanium tetrachloride; palladium on activated charcoal; In dichloromethane; acetic acid;
DOI:10.1021/jm00165a023