6-acetamido-2-fluorodibenzofuran

Base Information

Chemical Name:6-acetamido-2-fluorodibenzofuran
CAS No.:1386859-30-8
Molecular Formula:C₁₄H₁₀FNO₂
Molecular Weight:243.237
Hs Code.:

Synonyms:6-acetamido-2-fluorodibenzofuran

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Chemical Property of 6-acetamido-2-fluorodibenzofuran

Chemical Property:

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Technology Process of 6-acetamido-2-fluorodibenzofuran

There total 1 articles about 6-acetamido-2-fluorodibenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2713-29-3
2-iodo-4-fluorophenol

: 78887-39-5
3-Acetamidophenylboronic acid

: 1386859-30-8
6-acetamido-2-fluorodibenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / 1,4-dioxane; water / 100 °C / Inert atmosphere

2: oxygen; copper diacetate; Trimethylacetic acid / dimethyl sulfoxide / 17 h / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; oxygen; copper diacetate; potassium carbonate; Trimethylacetic acid; In 1,4-dioxane; water; dimethyl sulfoxide;
DOI:10.1055/s-0031-1290966

Reference yield:

: 1386859-30-8
6-acetamido-2-fluorodibenzofuran

: 7-fluoro-4-(3-bromophenyl)dibenzofuran

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide; water / ethanol; tetrahydrofuran / 18 h / Reflux

2.1: hydrogenchloride / water; 1,4-dioxane / 1 h / 20 °C / Reflux

2.2: 0.5 h / -10 - 5 °C

2.3: 4.5 h / 10 - 40 °C

3.1: n-butyllithium / tetrahydrofuran; acetone / 1 h / -60 - -50 °C / Inert atmosphere

3.2: 20 h / -45 - 20 °C / Inert atmosphere

3.3: 4 h / 10 - 20 °C / Inert atmosphere

4.1: potassium carbonate / toluene; ethanol; water / 0.5 h / 20 °C / Inert atmosphere

4.2: 2 h / Reflux

With hydrogenchloride; n-butyllithium; water; potassium carbonate; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; water; acetone; toluene;

Reference yield:

: 1386859-30-8
6-acetamido-2-fluorodibenzofuran

: 3-(7-fluorodibenzofuran-4-yl)phenylboronic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide; water / ethanol; tetrahydrofuran / 18 h / Reflux

2.1: hydrogenchloride / water; 1,4-dioxane / 1 h / 20 °C / Reflux

2.2: 0.5 h / -10 - 5 °C

2.3: 4.5 h / 10 - 40 °C

3.1: n-butyllithium / tetrahydrofuran; acetone / 1 h / -60 - -50 °C / Inert atmosphere

3.2: 20 h / -45 - 20 °C / Inert atmosphere

3.3: 4 h / 10 - 20 °C / Inert atmosphere

4.1: potassium carbonate / toluene; ethanol; water / 0.5 h / 20 °C / Inert atmosphere

4.2: 2 h / Reflux

5.1: n-butyllithium / tetrahydrofuran; acetone / 1 h / -60 - -50 °C / Inert atmosphere

5.2: 20 h / -45 - 20 °C / Inert atmosphere

5.3: 4 h / 10 - 20 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; water; potassium carbonate; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; water; acetone; toluene;