C₃₅H₅₄O₄Si₂

Base Information

Chemical Name:C₃₅H₅₄O₄Si₂
CAS No.:1261148-56-4
Molecular Formula:C₃₅H₅₄O₄Si₂
Molecular Weight:594.982
Hs Code.:

C<sub>35</sub>H<sub>54</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₅H₅₄O₄Si₂

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Chemical Property of C₃₅H₅₄O₄Si₂

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Technology Process of C₃₅H₅₄O₄Si₂

There total 12 articles about C₃₅H₅₄O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 994-30-9
triethylsilyl chloride

: 1261148-42-8
C₂₉H₄₀O₄Si

: 1261148-56-4
C₃₅H₅₄O₄Si₂

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 25 ℃; Inert atmosphere;
DOI:10.1021/ja109531d

Reference yield:

: 1227265-23-7
C₃₁H₃₆O₄Si

: 1261148-56-4
C₃₅H₅₄O₄Si₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: diethyl ether / 1 h / -78 °C / Inert atmosphere

2.1: 20 % Pd(OH)2/C; hydrogen / ethanol; ethyl acetate / 18 h / 25 °C

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 18 h / 25 °C / Inert atmosphere

4.1: dichloromethane / 4 h / 25 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / dichloromethane / -78 - 0 °C / Inert atmosphere

7.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.33 h / -20 °C / Molecular sieve; Inert atmosphere

7.2: 1 h / -20 °C / Inert atmosphere

8.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 9 h / 0 - 25 °C / Inert atmosphere

9.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

9.2: 1 h / -78 - 0 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

11.1: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 25 °C / Inert atmosphere

12.1: 1H-imidazole / dichloromethane / 0 - 25 °C / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2S,3S)-tartrate; [bis(acetoxy)iodo]benzene; 20 % Pd(OH)2/C; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene; 1.1: Grignard reaction / 7.1: Sharpless epoxidation / 7.2: Sharpless epoxidation / 9.1: Whiting reaction / 9.2: Whiting reaction;
DOI:10.1021/ja109531d

Reference yield:

: C₃₃H₅₀O₅Si₂

: 1261148-56-4
C₃₅H₅₄O₄Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / dichloromethane / -78 - 0 °C / Inert atmosphere

2.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.33 h / -20 °C / Molecular sieve; Inert atmosphere

2.2: 1 h / -20 °C / Inert atmosphere

3.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 9 h / 0 - 25 °C / Inert atmosphere

4.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

4.2: 1 h / -78 - 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

6.1: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 25 °C / Inert atmosphere

7.1: 1H-imidazole / dichloromethane / 0 - 25 °C / Inert atmosphere

With 1H-imidazole; titanium(IV) isopropylate; diethyl (2S,3S)-tartrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 2.1: Sharpless epoxidation / 2.2: Sharpless epoxidation / 4.1: Whiting reaction / 4.2: Whiting reaction;
DOI:10.1021/ja109531d