5-phenyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)pentanal

Base Information

Chemical Name:5-phenyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)pentanal
CAS No.:1311295-92-7
Molecular Formula:C₂₀H₃₁NO₂
Molecular Weight:317.472
Hs Code.:

Synonyms:5-phenyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)pentanal

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Chemical Property of 5-phenyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)pentanal

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Technology Process of 5-phenyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)pentanal

There total 3 articles about 5-phenyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)pentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 36884-28-3
5-phenyl-1-pentanal

: 1311295-92-7
5-phenyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)pentanal

Guidance literature:: With laccase; at 20 ℃; for 1h; pH=4.4; optical yield given as %ee; enantioselective reaction; aq. acetate buffer; Enzymatic reaction;
DOI:10.1021/ol2012956

Reference yield:

: 36884-28-3
5-phenyl-1-pentanal

: 26864-01-7
2,2,6,6-tetramethylpiperidin-1-oxoammonium chloride

: 2270-20-4
5-Phenylpentanoic acid

: 1311295-92-7
5-phenyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)pentanal

: C₂₀H₃₁NO₂

Guidance literature:: With resin supported Pro-D-Pro-Aib-Trp-Trp-(Leu)27.0-HN-CH₂-CH₂-PEG-PS; at 20 ℃; for 1h; pH=4.4; optical yield given as %ee; enantioselective reaction; aq. acetate buffer;
DOI:10.1021/ol2012956

Reference yield:

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 10521-91-2
5-phenylpentan-1-ol

: 1311295-92-7
5-phenyl-2-(2,2,6,6-tetramethylpiperidin-1-yloxy)pentanal

: C₂₀H₃₁NO₂

Guidance literature:: With [2,2]bipyridinyl; oxygen; copper(l) chloride; In tetrahydrofuran; water; at 20 ℃; for 36h; optical yield given as %ee; enantioselective reaction;
DOI:10.1039/c0cc02301a