pyridin-2-yl 2-O-(benzo-1-yl-3-carboxy)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:pyridin-2-yl 2-O-(benzo-1-yl-3-carboxy)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside
CAS No.:421593-93-3
Molecular Formula:C₄₀H₃₇NO₈S
Molecular Weight:691.802
Hs Code.:

Synonyms:pyridin-2-yl 2-O-(benzo-1-yl-3-carboxy)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Suppliers and Price of pyridin-2-yl 2-O-(benzo-1-yl-3-carboxy)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of pyridin-2-yl 2-O-(benzo-1-yl-3-carboxy)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of pyridin-2-yl 2-O-(benzo-1-yl-3-carboxy)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

There total 5 articles about pyridin-2-yl 2-O-(benzo-1-yl-3-carboxy)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2637-34-5,73018-10-7
2-Sulfanylpyridine

: 421593-93-3
pyridin-2-yl 2-O-(benzo-1-yl-3-carboxy)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / HgBr₂ / acetonitrile / 3.5 h / 60 °C

2: sodium methoxide / methanol / 2 h / 20 °C

3: toluene; pyridine / 2.5 h / 20 °C

4: diethyl ether; ethyl acetate

With sodium methylate; mercury dibromide; In pyridine; methanol; diethyl ether; ethyl acetate; toluene; acetonitrile;
DOI:10.1016/S0008-6215(01)00306-8

Reference yield:

: 68681-00-5
3,4,6-tri-O-benzyl-1,2-O-<1-(R)-methoxyethylidene>-β-D-mannopyranose

: 421593-93-3
pyridin-2-yl 2-O-(benzo-1-yl-3-carboxy)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / HgBr₂ / acetonitrile / 3.5 h / 60 °C

2: sodium methoxide / methanol / 2 h / 20 °C

3: toluene; pyridine / 2.5 h / 20 °C

4: diethyl ether; ethyl acetate

With sodium methylate; mercury dibromide; In pyridine; methanol; diethyl ether; ethyl acetate; toluene; acetonitrile;
DOI:10.1016/S0008-6215(01)00306-8

Reference yield:

: 164923-33-5
pyridin-2-yl 2-O-acetyl-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 421593-93-3
pyridin-2-yl 2-O-(benzo-1-yl-3-carboxy)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methoxide / methanol / 2 h / 20 °C

2: toluene; pyridine / 2.5 h / 20 °C

3: diethyl ether; ethyl acetate

With sodium methylate; In pyridine; methanol; diethyl ether; ethyl acetate; toluene;
DOI:10.1016/S0008-6215(01)00306-8