C₂₈H₂₈Cl₃NO₁₀

Base Information

Chemical Name:C₂₈H₂₈Cl₃NO₁₀
CAS No.:1262887-43-3
Molecular Formula:C₂₈H₂₈Cl₃NO₁₀
Molecular Weight:644.89
Hs Code.:

C<sub>28</sub>H<sub>28</sub>Cl<sub>3</sub>NO<sub>10</sub>

Synonyms:C₂₈H₂₈Cl₃NO₁₀

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Chemical Property of C₂₈H₂₈Cl₃NO₁₀

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Technology Process of C₂₈H₂₈Cl₃NO₁₀

There total 14 articles about C₂₈H₂₈Cl₃NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1262887-42-2
C₂₆H₂₈O₁₀

: 545-06-2
trichloroacetonitrile

: 1262887-43-3
C₂₈H₂₈Cl₃NO₁₀

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 10 - 20 ℃; for 2h; Inert atmosphere; Large scale;

Reference yield:

: 1,2;5,6-di-O-isopropylidene-β-D-mannofuranose

: 1262887-43-3
C₂₈H₂₈Cl₃NO₁₀

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil; tetrahydrofuran / 0.67 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 - 65 °C

2.1: acetic acid / 40 °C

3.1: tetrabutylammomium bromide; sodium periodate / water; dichloromethane / 3 h / 20 °C / Darkness

4.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 - -50 °C

4.2: 1.25 h / -78 - 20 °C

5.1: copper(II) oxide; copper dichloride / water; dichloromethane / 1.5 h / -78 - -50 °C

6.1: trifluoroacetic acid / water; dichloromethane / 20 °C

7.1: camphor-10-sulfonic acid / N,N-dimethyl-formamide; dichloromethane / 16 h / 0 - 20 °C

8.1: dmap; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 10 - 20 °C / Large scale

9.1: trifluoroacetic acid / 5 - 20 °C / Large scale

10.1: 1H-imidazole / dichloromethane / 3 h / -20 - 20 °C / Large scale

11.1: pyridine / dichloromethane / 3 h / -20 - 20 °C / Inert atmosphere; Large scale

12.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere; Large scale

13.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2 h / 10 - 20 °C / Inert atmosphere; Large scale

With pyridine; 1H-imidazole; dmap; sodium periodate; n-butyllithium; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; sodium hydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; copper(II) oxide; copper dichloride; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 100-39-0
benzyl bromide

: 1262887-43-3
C₂₈H₂₈Cl₃NO₁₀

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil; tetrahydrofuran / 0.67 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 - 65 °C

2.1: acetic acid / 40 °C

3.1: tetrabutylammomium bromide; sodium periodate / water; dichloromethane / 3 h / 20 °C / Darkness

4.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 - -50 °C

4.2: 1.25 h / -78 - 20 °C

5.1: copper(II) oxide; copper dichloride / water; dichloromethane / 1.5 h / -78 - -50 °C

6.1: trifluoroacetic acid / water; dichloromethane / 20 °C

7.1: camphor-10-sulfonic acid / N,N-dimethyl-formamide; dichloromethane / 16 h / 0 - 20 °C

8.1: dmap; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 10 - 20 °C / Large scale

9.1: trifluoroacetic acid / 5 - 20 °C / Large scale

10.1: 1H-imidazole / dichloromethane / 3 h / -20 - 20 °C / Large scale

11.1: pyridine / dichloromethane / 3 h / -20 - 20 °C / Inert atmosphere; Large scale

12.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere; Large scale

13.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2 h / 10 - 20 °C / Inert atmosphere; Large scale

With pyridine; 1H-imidazole; dmap; sodium periodate; n-butyllithium; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; sodium hydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; copper(II) oxide; copper dichloride; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;