(2S,9R)-2-Amino-11-[(benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-hydroxy-7-azaundecanoic Acid

Base Information

Chemical Name:(2S,9R)-2-Amino-11-[(benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-hydroxy-7-azaundecanoic Acid
CAS No.:189280-20-4
Molecular Formula:C₂₆H₃₅N₃O₇
Molecular Weight:501.58
Hs Code.:

Synonyms:(2S,9R)-2-Amino-11-[(benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-hydroxy-7-azaundecanoic Acid

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Chemical Property of (2S,9R)-2-Amino-11-[(benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-hydroxy-7-azaundecanoic Acid

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Technology Process of (2S,9R)-2-Amino-11-[(benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-hydroxy-7-azaundecanoic Acid

There total 5 articles about (2S,9R)-2-Amino-11-[(benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-hydroxy-7-azaundecanoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 189280-15-7
tert-butyl(2S,9R)-11-[(benzyloxycarbonyl)amino]-2-[(tert-butoxycarbonyl)amino]-9-hydroxy-7-(benzyloxycarbonyl)-7-azaundecanoate

: 189280-20-4
(2S,9R)-2-Amino-11-[(benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-hydroxy-7-azaundecanoic Acid

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; for 26h; Ambient temperature;
DOI:10.1021/jo970119z

Reference yield: 72.0%

: 189280-20-4
(2S,9R)-2-Amino-11-[(benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-hydroxy-7-azaundecanoic Acid

Guidance literature:

Reference yield:

: (2S,9R)-2-[(tert-Butoxycarbonyl)amino]-11-amino-9-hydroxy-7-azaundecanoic Acid tert-Butyl Ester, Diacetate Salt

: 189280-20-4
(2S,9R)-2-Amino-11-[(benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-hydroxy-7-azaundecanoic Acid

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / aq. KHCO₃ / diethyl ether / 4 h / Ambient temperature

2: 72 percent / trifluoroacetic acid, triethylsilane / CH₂Cl₂ / 39 h / Ambient temperature

With triethylsilane; potassium hydrogencarbonate; trifluoroacetic acid; In diethyl ether; dichloromethane;
DOI:10.1021/jm980389p