3a-fluoro-5-mesityl-8-methyl-1-tosyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Base Information

Chemical Name:3a-fluoro-5-mesityl-8-methyl-1-tosyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole
CAS No.:1334298-55-3
Molecular Formula:C₂₇H₂₉FN₂O₂S
Molecular Weight:464.604
Hs Code.:

Synonyms:3a-fluoro-5-mesityl-8-methyl-1-tosyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

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Chemical Property of 3a-fluoro-5-mesityl-8-methyl-1-tosyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

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Technology Process of 3a-fluoro-5-mesityl-8-methyl-1-tosyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

There total 15 articles about 3a-fluoro-5-mesityl-8-methyl-1-tosyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: C₂₅H₃₂N₂O₂

: 1334298-55-3
3a-fluoro-5-mesityl-8-methyl-1-tosyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Guidance literature:: C₂₅H₃₂N₂O₂; With 1,4-bis[(R)-(naphthalen-1-yl)[(2S)-1-(prop-2-en-1-yl)piperidin-2-yl]methoxy]phthalazine; sodium hydrogencarbonate; In acetone; at -78 ℃; for 0.25h;

With Selectfluor; In acetone; for 72h; enantioselective reaction;

Reference yield: 63.0%

: 1334298-39-3
N-(2-(5-mesityl-1-methyl-1H-indol-3-yl)ethyl)-4-methylbenzenesulfonamide

: 1334298-55-3
3a-fluoro-5-mesityl-8-methyl-1-tosyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Guidance literature:: With 1,4-bis[(R)-(naphthalen-1-yl)[(2S)-1-(prop-2-en-1-yl)piperidin-2-yl]methoxy]phthalazine; sodium hydrogencarbonate; Selectfluor; In acetone; at -78 ℃;
DOI:10.1002/adsc.201900814

Reference yield:

: 1334298-39-3
N-(2-(5-mesityl-1-methyl-1H-indol-3-yl)ethyl)-4-methylbenzenesulfonamide

: 3a-fluoro-5-mesityl-8-methyl-1-tosyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

: 1334298-55-3
3a-fluoro-5-mesityl-8-methyl-1-tosyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Guidance literature:: With potassium carbonate; N-fluorobis(benzenesulfon)imide; hydroquinidein 1,4-phthalazinediyl diether; In acetone; at -78 ℃; for 22h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201103151