N-tert-butoxycarbonyl-N'-(2-chlorophenyl)-N'-(4-fluorophenyl)hydrazine

Base Information

Chemical Name:N-tert-butoxycarbonyl-N'-(2-chlorophenyl)-N'-(4-fluorophenyl)hydrazine
CAS No.:1338369-65-5
Molecular Formula:C₁₇H₁₈ClFN₂O₂
Molecular Weight:336.794
Hs Code.:

Synonyms:N-tert-butoxycarbonyl-N'-(2-chlorophenyl)-N'-(4-fluorophenyl)hydrazine

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Chemical Property of N-tert-butoxycarbonyl-N'-(2-chlorophenyl)-N'-(4-fluorophenyl)hydrazine

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Technology Process of N-tert-butoxycarbonyl-N'-(2-chlorophenyl)-N'-(4-fluorophenyl)hydrazine

There total 6 articles about N-tert-butoxycarbonyl-N'-(2-chlorophenyl)-N'-(4-fluorophenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1338369-59-7
tert-butyl 2-(2-chlorophenyl)diazene-1-carboxylate

: 1765-93-1
4-fluoroboronic acid

: 1338369-65-5
N-tert-butoxycarbonyl-N'-(2-chlorophenyl)-N'-(4-fluorophenyl)hydrazine

Guidance literature:: tert-butyl 2-(2-chlorophenyl)diazene-1-carboxylate; 4-fluoroboronic acid; With copper(II) acetate monohydrate; In methanol; for 0.0833333h; Reflux; Inert atmosphere;

With silica gel; In methanol; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1055/s-0030-1260082

Reference yield:

: 823188-36-9
tert-butyl 2-(2-chlorophenyl)hydrazine-1-carboxylate

: 1338369-65-5
N-tert-butoxycarbonyl-N'-(2-chlorophenyl)-N'-(4-fluorophenyl)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; N-Bromosuccinimide / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: copper(II) acetate monohydrate / methanol / 0.08 h / Reflux; Inert atmosphere

2.2: 0.08 h / 20 °C / Inert atmosphere

With pyridine; N-Bromosuccinimide; copper(II) acetate monohydrate; In methanol; dichloromethane;
DOI:10.1055/s-0030-1260082

Reference yield:

: 857595-49-4
o-chloronitroaniline

: 1338369-65-5
N-tert-butoxycarbonyl-N'-(2-chlorophenyl)-N'-(4-fluorophenyl)hydrazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; tin(II) chloride dihdyrate; water / 2.5 h / 0 °C / Inert atmosphere

2.1: tetrahydrofuran / 20 °C / Inert atmosphere

3.1: pyridine; N-Bromosuccinimide / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4.1: copper(II) acetate monohydrate / methanol / 0.08 h / Reflux; Inert atmosphere

4.2: 0.08 h / 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; N-Bromosuccinimide; tin(II) chloride dihdyrate; water; copper(II) acetate monohydrate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1055/s-0030-1260082