C₂₁H₂₇BrN₄O₅

Base Information

Chemical Name:C₂₁H₂₇BrN₄O₅
CAS No.:1612854-68-8
Molecular Formula:C₂₁H₂₇BrN₄O₅
Molecular Weight:495.373
Hs Code.:

C<sub>21</sub>H<sub>27</sub>BrN<sub>4</sub>O<sub>5</sub>

Synonyms:C₂₁H₂₇BrN₄O₅

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Chemical Property of C₂₁H₂₇BrN₄O₅

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Technology Process of C₂₁H₂₇BrN₄O₅

There total 7 articles about C₂₁H₂₇BrN₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1296797-09-5
C₁₄H₂₂N₂O₅

: 16313-66-9
5-bromoanthranilamide

: 1612854-68-8
C₂₁H₂₇BrN₄O₅

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; for 8h; Inert atmosphere;

Reference yield:

: 52727-57-8
5-bromo-2-aminobenzoic acid methyl ester

: 1612854-68-8
C₂₁H₂₇BrN₄O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; water / tetrahydrofuran / 60 °C

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / 20 °C

2.2: 0 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 8 h / 0 - 20 °C / Inert atmosphere

With water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; sodium hydroxide; In tetrahydrofuran;

Reference yield:

: 5794-88-7
5-Bromo-2-aminobenzoic acid

: 1612854-68-8
C₂₁H₂₇BrN₄O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / 20 °C

1.2: 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 8 h / 0 - 20 °C / Inert atmosphere

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran;