allyl 2,4-di-O-benzoyl-3-O-methyl-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Base Information

Chemical Name:allyl 2,4-di-O-benzoyl-3-O-methyl-6-O-(4-methoxybenzyl)-β-D-glucopyranoside
CAS No.:136737-59-2
Molecular Formula:C₃₂H₃₄O₉
Molecular Weight:562.617
Hs Code.:

Synonyms:allyl 2,4-di-O-benzoyl-3-O-methyl-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2,4-di-O-benzoyl-3-O-methyl-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

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Technology Process of allyl 2,4-di-O-benzoyl-3-O-methyl-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

There total 9 articles about allyl 2,4-di-O-benzoyl-3-O-methyl-6-O-(4-methoxybenzyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 98-88-4
benzoyl chloride

: 136737-58-1
allyl 2-O-benzoyl-3-O-methyl-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

: 136737-59-2
allyl 2,4-di-O-benzoyl-3-O-methyl-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Guidance literature:: With pyridine; for 2h; Ambient temperature;
DOI:10.1016/0008-6215(92)84172-O

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 136737-59-2
allyl 2,4-di-O-benzoyl-3-O-methyl-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / p-TsOH / dimethylformamide / 2 h / 50 °C

2: 86 percent / pyridine / 2 h / Ambient temperature

3: 70 percent / TFA, sodium cyanoborohydride, 3 Angstroem molecular sieves / dimethylformamide / 18 h / Ambient temperature

4: 93 percent / pyridine / 2 h / Ambient temperature

With pyridine; 3 A molecular sieve; sodium cyanoborohydride; toluene-4-sulfonic acid; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(92)84172-O

Reference yield:

: 129192-93-4
allyl 2,4,6-tri-O-acetyl-3-O-methyl-β-D-glucopyranoside

: 136737-59-2
allyl 2,4-di-O-benzoyl-3-O-methyl-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / NaOMe / methanol / 16 h

2: 82 percent / p-TsOH / dimethylformamide / 2 h / 50 °C

3: 86 percent / pyridine / 2 h / Ambient temperature

4: 70 percent / TFA, sodium cyanoborohydride, 3 Angstroem molecular sieves / dimethylformamide / 18 h / Ambient temperature

5: 93 percent / pyridine / 2 h / Ambient temperature

With pyridine; 3 A molecular sieve; sodium methylate; sodium cyanoborohydride; toluene-4-sulfonic acid; trifluoroacetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(92)84172-O