2,2′-bis[phenylmethylene]carbonimidic dihydrazide monohydrochloride

Base Information

• Chemical Name: 2,2′-bis[phenylmethylene]carbonimidic dihydrazide monohydrochloride
• CAS No.: 72463-09-3
• Molecular Formula: C₁₅H₁₅N₅*ClH
• Molecular Weight: 301.779
• Mol file: 72463-09-3.mol

Synonyms:2,2′-bis[phenylmethylene]carbonimidic dihydrazide monohydrochloride

Chemical Property of 2,2′-bis[phenylmethylene]carbonimidic dihydrazide monohydrochloride

Chemical Property:

Purity/Quality:

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Technology Process of 2,2′-bis[phenylmethylene]carbonimidic dihydrazide monohydrochloride

There total 2 articles about 2,2′-bis[phenylmethylene]carbonimidic dihydrazide monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,3-diaminoguanidine hydrochloride (36062-19-8,38360-74-6) + benzaldehyde (100-52-7) → 2,2′-bis[phenylmethylene]carbonimidic dihydrazide monohydrochloride (72463-09-3)

Guidance literature:

In ethanol; for 16h; Reflux;

DOI:10.1021/acsinfecdis.1c00001

Reference yield:

1,3-diaminoguanidine hydrochloride (36062-19-8,38360-74-6) + benzaldehyde (100-52-7) + 2-Fluorobenzaldehyde (446-52-6) → 2,2′-bis[(2-fluorophenyl)methylene]carbonimidic dihydrazide monohydrochloride + 2,2′-bis[phenylmethylene]carbonimidic dihydrazide monohydrochloride (72463-09-3) + 2-(phenylmethylene)-2'-[(2-fluorophenyl)methylene]-carbonimidic dihydrazide hydrochloride

Guidance literature:

In ethanol; for 16h; Reflux;

DOI:10.1021/acsinfecdis.1c00001

Reference yield:

2,2′-bis[phenylmethylene]carbonimidic dihydrazide monohydrochloride (72463-09-3) → 3,5,3',5'-tetraphenyl-1,1'-carboximidoyl-di-formazan

Guidance literature:

With potassium hydroxide; anschliessend mit wss. Benzoldiazoniumchlorid;

upstream raw materials:

1,3-diaminoguanidine hydrochloride

benzaldehyde

2-Fluorobenzaldehyde