N-(4-cyano-2-ethylsulfanyl-5-trifluoromethyl-phenyl)-2-methyl-acrylamide

Base Information

Chemical Name:N-(4-cyano-2-ethylsulfanyl-5-trifluoromethyl-phenyl)-2-methyl-acrylamide
CAS No.:888073-00-5
Molecular Formula:C₁₄H₁₃F₃N₂OS
Molecular Weight:314.331
Hs Code.:

Synonyms:N-(4-cyano-2-ethylsulfanyl-5-trifluoromethyl-phenyl)-2-methyl-acrylamide

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Chemical Property of N-(4-cyano-2-ethylsulfanyl-5-trifluoromethyl-phenyl)-2-methyl-acrylamide

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Technology Process of N-(4-cyano-2-ethylsulfanyl-5-trifluoromethyl-phenyl)-2-methyl-acrylamide

There total 4 articles about N-(4-cyano-2-ethylsulfanyl-5-trifluoromethyl-phenyl)-2-methyl-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 888072-99-9
4-cyano-5-trifluoromethyl-2-ethylsulfanyl-aniline

: 79-41-4,25087-26-7,50867-57-7
poly(methacrylic acid)

: 888073-00-5
N-(4-cyano-2-ethylsulfanyl-5-trifluoromethyl-phenyl)-2-methyl-acrylamide

Guidance literature:: poly(methacrylic acid); With thionyl chloride; In N,N-dimethyl acetamide; at 0 ℃; for 0.5h;

4-cyano-5-trifluoromethyl-2-ethylsulfanyl-aniline; In N,N-dimethyl acetamide; Further stages.;
DOI:10.1021/jm0613976

Reference yield:

: 852569-35-8
4-amino-5-iodo-2-(trifluoromethyl)benzonitrile

: 888073-00-5
N-(4-cyano-2-ethylsulfanyl-5-trifluoromethyl-phenyl)-2-methyl-acrylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 90 percent / K₂CO₃ / CuI / ethanol / Heating

2.1: thionyl chloride / N,N-dimethyl-acetamide / 0.5 h / 0 °C

2.2: 56 percent / N,N-dimethyl-acetamide

With thionyl chloride; potassium carbonate; copper(l) iodide; In ethanol; N,N-dimethyl acetamide;
DOI:10.1021/jm0613976