C₄₈H₆₃N₃O₆

Base Information

Chemical Name:C₄₈H₆₃N₃O₆
CAS No.:1280737-10-1
Molecular Formula:C₄₈H₆₃N₃O₆
Molecular Weight:778.045
Hs Code.:

C<sub>48</sub>H<sub>63</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:C₄₈H₆₃N₃O₆

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Chemical Property of C₄₈H₆₃N₃O₆

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Technology Process of C₄₈H₆₃N₃O₆

There total 8 articles about C₄₈H₆₃N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1280736-93-7
C₅₁H₆₁N₃O₆

: 1280737-10-1
C₄₈H₆₃N₃O₆

Guidance literature:: With 20 % Pd(OH)2/C; hydrogen; In methanol; at 20 ℃; for 16h; under 760.051 Torr;
DOI:10.1016/j.tetasy.2010.12.007

Reference yield:

: 820236-58-6
t-butyl (1S,2S,3S)-3-benzyl-2-aminocyclopentane-1-carboxylate

: 1280737-10-1
C₄₈H₆₃N₃O₆

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 16 h / 20 °C / Inert atmosphere

4: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 20 °C / 3800.26 Torr

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 16 h / 20 °C / Inert atmosphere

6: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 20 °C / 760.05 Torr

With 20 % Pd(OH)2/C; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform;
DOI:10.1016/j.tetasy.2010.12.007

Reference yield:

: 820236-49-5
tert-butyl (1S,2S,3S,αS)-3-benzyl-2-(N-benzyl-N-α-methylbenzylamino)-cyclopentane-1-carboxylate

: 1280737-10-1
C₄₈H₆₃N₃O₆

Guidance literature:: Multi-step reaction with 7 steps

1: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 16 h / 20 °C / 3800.26 Torr

2: triethylamine / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 16 h / 20 °C / Inert atmosphere

5: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 20 °C / 3800.26 Torr

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform / 16 h / 20 °C / Inert atmosphere

7: 20 % Pd(OH)2/C; hydrogen / methanol / 16 h / 20 °C / 760.05 Torr

With 20 % Pd(OH)2/C; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform; ethyl acetate;
DOI:10.1016/j.tetasy.2010.12.007