2,4(1H,3H)-Pyrimidinedione,6-(2,3-dihydroxypropyl)-5-methyl-(9CI)

Base Information

Chemical Name:2,4(1H,3H)-Pyrimidinedione,6-(2,3-dihydroxypropyl)-5-methyl-(9CI)
CAS No.:820966-05-0
Molecular Formula:C8H12 N2 O4
Molecular Weight:200.19
Hs Code.:
Mol file:820966-05-0.mol

Synonyms:2,4(1H,3H)-Pyrimidinedione,6-(2,3-dihydroxypropyl)-5-methyl-(9CI)

Suppliers and Price of 2,4(1H,3H)-Pyrimidinedione,6-(2,3-dihydroxypropyl)-5-methyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 2,4(1H,3H)-Pyrimidinedione,6-(2,3-dihydroxypropyl)-5-methyl-(9CI)

Chemical Property:

PSA：106.18000
LogP:-1.73270

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4(1H,3H)-Pyrimidinedione,6-(2,3-dihydroxypropyl)-5-methyl-(9CI)

There total 5 articles about 2,4(1H,3H)-Pyrimidinedione,6-(2,3-dihydroxypropyl)-5-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: acetic acid 1-hydroxymethyl-2-(5-methyl-2,6-dioxo-1,2,3,6-tetrahydro-pyrimidin-4-yl)-ethyl ester

: 820966-05-0
6-(2,3-dihydroxypropyl)-5-methyl-(1H,3H)-pyrimidine-2,4-dione

Guidance literature:: With sodium hydrogencarbonate; In methanol; dichloromethane;
DOI:10.1081/NCN-200033914

Reference yield:

: 856766-74-0
6-(3-benzyloxy-2-hydroxypropyl)-2,4-dimethoxy-5-methylpyrimidine

: 820966-05-0
6-(2,3-dihydroxypropyl)-5-methyl-(1H,3H)-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 10 h / Heating

2: 193 mg / acetic chloride; water / 20 °C

3: boron trichloride / CH₂Cl₂ / -75 - -40 °C

4: 35 mg / sodium hydrogen carbonate / methanol; CH₂Cl₂

With water; boron trichloride; sodium hydrogencarbonate; acetyl chloride; In methanol; dichloromethane;
DOI:10.1081/NCN-200033914

Reference yield:

: 856766-75-1
6-(2-acetoxy-3-benzyloxypropyl)-5-methyl-(1H,3H)-pyrimidine-2,4-dione

: 820966-05-0
6-(2,3-dihydroxypropyl)-5-methyl-(1H,3H)-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: boron trichloride / CH₂Cl₂ / -75 - -40 °C

2: 35 mg / sodium hydrogen carbonate / methanol; CH₂Cl₂

With boron trichloride; sodium hydrogencarbonate; In methanol; dichloromethane;
DOI:10.1081/NCN-200033914