N¹,N¹-diisopropyl-N²-(4-methylbenzenesulfonyl)-2-cyclohexylacetamidine

Base Information

Chemical Name:N¹,N¹-diisopropyl-N²-(4-methylbenzenesulfonyl)-2-cyclohexylacetamidine
CAS No.:1448532-91-9
Molecular Formula:C₂₁H₃₄N₂O₂S
Molecular Weight:378.579
Hs Code.:

N<SUP>1</SUP>,N<SUP>1</SUP>-diisopropyl-N<SUP>2</SUP>-(4-methylbenzenesulfonyl)-2-cyclohexylacetamidine

Synonyms:N¹,N¹-diisopropyl-N²-(4-methylbenzenesulfonyl)-2-cyclohexylacetamidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹,N¹-diisopropyl-N²-(4-methylbenzenesulfonyl)-2-cyclohexylacetamidine

Chemical Property:

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Technology Process of N¹,N¹-diisopropyl-N²-(4-methylbenzenesulfonyl)-2-cyclohexylacetamidine

There total 3 articles about N¹,N¹-diisopropyl-N²-(4-methylbenzenesulfonyl)-2-cyclohexylacetamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 941-55-9
4-toluenesulfonyl azide

: 931-48-6
2-cyclohexylacetylene

: 108-18-9
diisopropylamine

: 1448532-91-9
N¹,N¹-diisopropyl-N²-(4-methylbenzenesulfonyl)-2-cyclohexylacetamidine

Guidance literature:: With Cu(at)C, generated by pyrolysis of Cu₃(1,3,5-benzenetricarboxylate)₂; In acetonitrile; at 25 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2016.07.085

Reference yield: 94.0%

: 1448532-91-9
N¹,N¹-diisopropyl-N²-(4-methylbenzenesulfonyl)-2-cyclohexylacetamidine

Guidance literature:: With heterogeneous copper catalyst; In acetonitrile; at 25 ℃; for 3h; Inert atmosphere;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1448532-91-9
N¹,N¹-diisopropyl-N²-(4-methylbenzenesulfonyl)-2-cyclohexylacetamidine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / acetone / 0 °C

2: Cu₂I₂(benzene-1,3,5-triyl triisonicotinate) / acetonitrile / 2 h / 20 °C / Inert atmosphere

With sodium azide; Cu₂I₂(benzene-1,3,5-triyl triisonicotinate); In acetone; acetonitrile;
DOI:10.1021/ic4012229