sodium 2-(4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butylcyclohex-1-enyl)phenyl]ethyl}benzoylamino)ethanesulfonate

Base Information

Chemical Name:sodium 2-(4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butylcyclohex-1-enyl)phenyl]ethyl}benzoylamino)ethanesulfonate
CAS No.:1046303-42-7
Molecular Formula:C₃₄H₃₈BrN₂O₅S*Na
Molecular Weight:689.646
Hs Code.:

Synonyms:sodium 2-(4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butylcyclohex-1-enyl)phenyl]ethyl}benzoylamino)ethanesulfonate

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Chemical Property of sodium 2-(4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butylcyclohex-1-enyl)phenyl]ethyl}benzoylamino)ethanesulfonate

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Technology Process of sodium 2-(4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butylcyclohex-1-enyl)phenyl]ethyl}benzoylamino)ethanesulfonate

There total 6 articles about sodium 2-(4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butylcyclohex-1-enyl)phenyl]ethyl}benzoylamino)ethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-35-7
Tau

: 1207989-31-8
C₃₂H₃₄BrNO₃

: 1046303-42-7
sodium 2-(4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butylcyclohex-1-enyl)phenyl]ethyl}benzoylamino)ethanesulfonate

Guidance literature:: Tau; C₃₂H₃₄BrNO₃; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

With hydrogenchloride; In water; ethyl acetate; N,N-dimethyl-formamide;

With sodium hydroxide; In methanol; water;

Reference yield:

: 107-35-7
Tau

: 1207989-28-3
4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butyl-cyclohex-1-enyl)phenyl]ethyl}benzoic acid methyl ester

: 1046303-42-7
sodium 2-(4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butylcyclohex-1-enyl)phenyl]ethyl}benzoylamino)ethanesulfonate

Guidance literature:: 4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butyl-cyclohex-1-enyl)phenyl]ethyl}benzoic acid methyl ester; With water; lithium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 16h;

Tau; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

With sodium hydroxide; In MeOH;

Reference yield:

: 1878-68-8
2-(4-bromophenyl)-acetic acid

: 1046303-42-7
sodium 2-(4-{2-(4-bromophenylcarbamoyl)-2-[4-(4-tert-butylcyclohex-1-enyl)phenyl]ethyl}benzoylamino)ethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 - 10 °C / Inert atmosphere

1.2: 0.25 h / -60 °C

2.1: dichlorobis(tri-O-tolylphosphine)palladium; sodium carbonate / tetrahydrofuran; ethanol; water / 1 h / 125 °C

2.2: 1 h / 100 °C

2.3: 1 h / 100 °C

3.1: lithium hydroxide; water / tetrahydrofuran; methanol / 16 h / 20 °C

3.2: 16 h / 20 °C

With dichlorobis(tri-O-tolylphosphine)palladium; water; sodium carbonate; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; water;