1-methyl-2-[2-(phenyltriethylsiloxymethyl)-1-cyclohexenyl]-1H-imidazole

Base Information

Chemical Name:1-methyl-2-[2-(phenyltriethylsiloxymethyl)-1-cyclohexenyl]-1H-imidazole
CAS No.:1161621-84-6
Molecular Formula:C₂₃H₃₄N₂OSi
Molecular Weight:382.621
Hs Code.:

Synonyms:1-methyl-2-[2-(phenyltriethylsiloxymethyl)-1-cyclohexenyl]-1H-imidazole

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Chemical Property of 1-methyl-2-[2-(phenyltriethylsiloxymethyl)-1-cyclohexenyl]-1H-imidazole

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Technology Process of 1-methyl-2-[2-(phenyltriethylsiloxymethyl)-1-cyclohexenyl]-1H-imidazole

There total 2 articles about 1-methyl-2-[2-(phenyltriethylsiloxymethyl)-1-cyclohexenyl]-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 617-86-7
triethylsilane

: 127782-72-3
2-cyclohexenyl-1-methylimidazole

: 100-52-7
benzaldehyde

: 1161621-84-6
1-methyl-2-[2-(phenyltriethylsiloxymethyl)-1-cyclohexenyl]-1H-imidazole

Guidance literature:: With bromotricarbonyl(tetrahydrofuran)rhenium(I) dimer; In toluene; at 115 ℃; for 24h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol900962v

Reference yield: 38.0%

: 617-86-7
triethylsilane

: 127782-72-3
2-cyclohexenyl-1-methylimidazole

: 100-51-6,185532-71-2
benzyl alcohol

: 1161621-84-6
1-methyl-2-[2-(phenyltriethylsiloxymethyl)-1-cyclohexenyl]-1H-imidazole

Guidance literature:: benzyl alcohol; With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; (E)-3-methylpent-3-en-2-one; potassium carbonate; In toluene; at 150 ℃; for 18h;

triethylsilane; 2-cyclohexenyl-1-methylimidazole; With [ReBr(CO)3(thf)]2; In toluene; at 115 ℃; for 24h; Molecular sieve;
DOI:10.1055/s-0030-1259040