(Z)-1-{2-(tri-p-tolylstannyl)vinyl}-1-cyclohexanol

Base Information

Chemical Name:(Z)-1-{2-(tri-p-tolylstannyl)vinyl}-1-cyclohexanol
CAS No.:156217-15-1
Molecular Formula:C₂₉H₃₄OSn
Molecular Weight:517.298
Hs Code.:

Synonyms:(Z)-1-{2-(tri-p-tolylstannyl)vinyl}-1-cyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-{2-(tri-p-tolylstannyl)vinyl}-1-cyclohexanol

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Technology Process of (Z)-1-{2-(tri-p-tolylstannyl)vinyl}-1-cyclohexanol

There total 1 articles about (Z)-1-{2-(tri-p-tolylstannyl)vinyl}-1-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 796-14-5
tri(p-tolyl)tin hydride

: 78-27-3
1-Ethynylcyclohexan-1-ol

: 156217-15-1
(Z)-1-{2-(tri-p-tolylstannyl)vinyl}-1-cyclohexanol

Guidance literature:: In benzene; addn. of benzene and dibenzoyl peroxide to a mixt. of (C6H5)3SnH and ethinylcyclohexanol under N2; stirring, 20h; evapn.; crystn. (ethanol); filtration; elem. anal.;

Reference yield: 84.0%

: 156217-15-1
(Z)-1-{2-(tri-p-tolylstannyl)vinyl}-1-cyclohexanol

: 156217-17-3
(Z)-1-{2-(p-tolyldibromostannyl)vinyl}-1-cyclohexanol

Guidance literature:: With Br₂; In chloroform; dropwise addn. of Br2 soln. to Sn compd. soln. (molar ratio 2:1) with stirring; keeping at -10°C, 5h; evapn.; crystn. (cyclohexane); elem. anal.;

Reference yield: 76.0%

: 156217-15-1
(Z)-1-{2-(tri-p-tolylstannyl)vinyl}-1-cyclohexanol

: 7790-99-0
Iodine monochloride

: 156217-16-2
(Z)-1-{2-(p-tolyldichlorostannyl)vinyl}-1-cyclohexanol

Guidance literature:: In chloroform; dropwise addn. of ICl soln. to Sn compd. soln. (molar ratio 2:1) with stirring; keeping at 0°C, 5h; evapn.; crystn. (cyclohexane/CCl4); elem. anal.;