Technology Process of C38H50N2O9Si
There total 11 articles about C38H50N2O9Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 86 percent / diisobutylaluminium hydride / CH2Cl2 / 1.5 h / -78 °C
2: 100 percent / potassium hexamethyldisilazide / diethyl ether / -78 - 20 °C
3: 51 percent / CsCO3 / 1,2-dimethoxy-ethane / 15 h / 0 °C
4: 49 percent / boric acid; hydrogen / Raney nickel / ethanol; H2O / 22 h / 20 °C
5: diethylmethoxyborane; NaBH4 / tetrahydrofuran / 15 h / -78 °C
6: 97 percent / para-toluenesulfonic acid / 2 h / 20 °C
With
sodium tetrahydroborate; diethyl methoxy borane; hydrogen; boric acid; potassium hexamethylsilazane; diisobutylaluminium hydride; toluene-4-sulfonic acid;
nickel;
In
tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; ethanol; dichloromethane; water;
2: Wittig methylenation;
DOI:10.1002/chem.200700033
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 100 percent / potassium hexamethyldisilazide / diethyl ether / -78 - 20 °C
2: 51 percent / CsCO3 / 1,2-dimethoxy-ethane / 15 h / 0 °C
3: 49 percent / boric acid; hydrogen / Raney nickel / ethanol; H2O / 22 h / 20 °C
4: diethylmethoxyborane; NaBH4 / tetrahydrofuran / 15 h / -78 °C
5: 97 percent / para-toluenesulfonic acid / 2 h / 20 °C
With
sodium tetrahydroborate; diethyl methoxy borane; hydrogen; boric acid; potassium hexamethylsilazane; toluene-4-sulfonic acid;
nickel;
In
tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; ethanol; water;
1: Wittig methylenation;
DOI:10.1002/chem.200700033
