Technology Process of C13H12ClNO2
There total 7 articles about C13H12ClNO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
acetone;
at 20 ℃;
for 14h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tert-butyl chloroformate; triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
2: trifluoroacetic anhydride; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
3: toluene-4-sulfonic acid / acetone / 14 h / 20 °C / Inert atmosphere
With
toluene-4-sulfonic acid; tert-butyl chloroformate; triethylamine; trifluoroacetic anhydride;
In
tetrahydrofuran; dichloromethane; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic anhydride; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: toluene-4-sulfonic acid / acetone / 14 h / 20 °C / Inert atmosphere
With
toluene-4-sulfonic acid; triethylamine; trifluoroacetic anhydride;
In
dichloromethane; acetone;