BrC₆H₄C₄HNCHO₂CCH₃CH₂(HgO₂CCH₃)2COCF₃

Base Information

• Chemical Name: BrC₆H₄C₄HNCHO₂CCH₃CH₂(HgO₂CCH₃)2COCF₃
• CAS No.: 1372648-19-5
• Molecular Formula: C₂₀H₁₇BrF₃Hg₂NO₇
• Molecular Weight: 921.437
• Mol file: 1372648-19-5.mol

Synonyms:BrC₆H₄C₄HNCHO₂CCH₃CH₂(HgO₂CCH₃)2COCF₃

Chemical Property of BrC₆H₄C₄HNCHO₂CCH₃CH₂(HgO₂CCH₃)2COCF₃

Chemical Property:

Purity/Quality:

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Technology Process of BrC₆H₄C₄HNCHO₂CCH₃CH₂(HgO₂CCH₃)2COCF₃

There total 1 articles about BrC₆H₄C₄HNCHO₂CCH₃CH₂(HgO₂CCH₃)2COCF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-(5-(4-bromophenyl)-N-vinylpyrrol-2-yl)-2,2,2-trifluoroethanone (72607-13-7) + mercury(II) diacetate (1600-27-7) → BrC6H4C4H2NCHO2CCH3CH2HgO2CCH3COCF3 (1372648-10-6) + BrC6H4C4HNCHO2CCH3CH2(HgO2CCH3)2COCF3 (1372648-19-5)

Guidance literature:

In acetonitrile; byproducts: CH3COOH; by a react. in dry CH3CN at 60°C for 12 h; 3-fold excess of Hg(OAc)2;

DOI:10.1039/c2dt12393b

Reference yield: 96.0%

BrC6H4C4HNCHO2CCH3CH2(HgO2CCH3)2COCF3 (1372648-19-5) → 1-(5-(4-bromophenyl)-1-vinyl-1H-pyrrol-2-yl)-2,2,2-trifluoroethanol (1372648-24-2)

Guidance literature:

With sodium tetrahydroborate; In water; acetonitrile; at 20 ℃; for 0.5h;

DOI:10.1039/c2dt12393b

upstream raw materials:

1-(5-(4-bromophenyl)-N-vinylpyrrol-2-yl)-2,2,2-trifluoroethanone

mercury(II) diacetate

Downstream raw materials:

1-(5-(4-bromophenyl)-1-vinyl-1H-pyrrol-2-yl)-2,2,2-trifluoroethanol