[1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diallyl ester

Base Information

Chemical Name:[1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diallyl ester
CAS No.:870193-92-3
Molecular Formula:C₁₆H₂₀ClO₃PS
Molecular Weight:358.826
Hs Code.:

Synonyms:[1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diallyl ester

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Chemical Property of [1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diallyl ester

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Technology Process of [1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diallyl ester

There total 4 articles about [1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diallyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 870193-94-5
[1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diethyl ester

: 107-18-6
allyl alcohol

: 870193-92-3
[1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diallyl ester

Guidance literature:: [1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diethyl ester; With oxalyl dichloride; trimethylsilyl bromide;

allyl alcohol;
DOI:10.1021/jo051206r

Reference yield:

: 10419-77-9
diethyl iodomethanephosphonate

: 870193-92-3
[1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diallyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol

2: 73 percent / n-BuLi

3: 27 percent / TMSBr; (COCl)2

With potassium hydroxide; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; In ethanol;
DOI:10.1021/jo051206r

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 870193-92-3
[1-(4-chloro-phenylsulfanyl)-but-3-enyl]-phosphonic acid diallyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol

2: 73 percent / n-BuLi

3: 27 percent / TMSBr; (COCl)2

With potassium hydroxide; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; In ethanol;
DOI:10.1021/jo051206r