4-acetoxy-3-isopentylbenzoic acid

Base Information

Chemical Name:4-acetoxy-3-isopentylbenzoic acid
CAS No.:1432-15-1
Molecular Formula:C₁₄H₁₈O₄
Molecular Weight:250.295
Hs Code.:

Synonyms:4-acetoxy-3-isopentylbenzoic acid

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Chemical Property of 4-acetoxy-3-isopentylbenzoic acid

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Technology Process of 4-acetoxy-3-isopentylbenzoic acid

There total 7 articles about 4-acetoxy-3-isopentylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100256-92-6
4-hydroxy-3-isopentylbenzoic acid

: 108-24-7
acetic anhydride

: 1432-15-1
4-acetoxy-3-isopentylbenzoic acid

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; Cooling with ice;
DOI:10.1021/acs.jmedchem.0c01564

Reference yield:

: 110-86-1
pyridine

: 108-24-7
acetic anhydride

: 29826-16-2
7-(O³-carbamoyl-5,O⁴-dimethyl-β-L-lyxo-6-deoxy-hexopyranosyloxy)-4-hydroxy-3-(4-hydroxy-3-isopentyl-benzoylamino)-8-methyl-coumarin

: 1432-15-1
4-acetoxy-3-isopentylbenzoic acid

: 7255-56-3,116697-40-6
7-(O²-acetyl-O³-carbamoyl-5,O⁴-dimethyl-β-L-lyxo-6-deoxy-hexopyranosyloxy)-2,6-dimethyl-chromeno[3,4-d]oxazol-4-one

Guidance literature:: DOI:10.1021/ja01571a047

Reference yield:

: methyl 4-(benzyloxy)-3-(3-methylbut-1-en-1-yl)benzoate

: 1432-15-1
4-acetoxy-3-isopentylbenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; palladium 10% on activated carbon / methanol / 6 h / 20 °C

2: potassium hydroxide / methanol; water; tetrahydrofuran / 5 h / Reflux

3: pyridine / dichloromethane / 0 - 20 °C / Cooling with ice

With pyridine; palladium 10% on activated carbon; hydrogen; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/acs.jmedchem.0c01564