Decanethioic acid S-{(R)-1-benzyloxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl} ester

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Chemical Name:Decanethioic acid S-{(R)-1-benzyloxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl} ester
CAS No.:161392-12-7
Molecular Formula:C₄₀H₄₈O₄S
Molecular Weight:624.885
Hs Code.:

Synonyms:Decanethioic acid S-{(R)-1-benzyloxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl} ester

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Chemical Property of Decanethioic acid S-{(R)-1-benzyloxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl} ester

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Technology Process of Decanethioic acid S-{(R)-1-benzyloxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl} ester

There total 7 articles about Decanethioic acid S-{(R)-1-benzyloxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56552-80-8
(R)-3-benzyloxy-1,2-propanediol

: 161392-12-7
Decanethioic acid S-{(R)-1-benzyloxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl} ester

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / tetrahydrofuran / 14 h / 25 °C

2: pyridine / CH₂Cl₂ / 14 h / 25 °C

3: dimethylformamide / 16 h / 80 °C

4: NaBH₄ / ethanol / 1 h / 55 °C

5: pyridine / 14 h / 25 °C

With pyridine; sodium tetrahydroborate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009

Reference yield:

: 100-39-0
benzyl bromide

: 161392-12-7
Decanethioic acid S-{(R)-1-benzyloxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl} ester

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) NaH / 1.) DMF, 25 deg C, 30 min, 2.) DMF, 0 deg C to 25 deg C, 4 h

2: 5 N HCl / methanol / 2 h / Heating

3: pyridine / tetrahydrofuran / 14 h / 25 °C

4: pyridine / CH₂Cl₂ / 14 h / 25 °C

5: dimethylformamide / 16 h / 80 °C

6: NaBH₄ / ethanol / 1 h / 55 °C

7: pyridine / 14 h / 25 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009

Reference yield:

: (S)-1-Benzyloxy-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propan-2-ol

: 161392-12-7
Decanethioic acid S-{(R)-1-benzyloxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethyl} ester

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / CH₂Cl₂ / 14 h / 25 °C

2: dimethylformamide / 16 h / 80 °C

3: NaBH₄ / ethanol / 1 h / 55 °C

4: pyridine / 14 h / 25 °C

With pyridine; sodium tetrahydroborate; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009