C₄₆H₆₀O₅SSi

Base Information

Chemical Name:C₄₆H₆₀O₅SSi
CAS No.:1028432-63-4
Molecular Formula:C₄₆H₆₀O₅SSi
Molecular Weight:753.131
Hs Code.:

C<sub>46</sub>H<sub>60</sub>O<sub>5</sub>SSi

Synonyms:C₄₆H₆₀O₅SSi

Suppliers and Price of C₄₆H₆₀O₅SSi

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₆H₆₀O₅SSi

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₆H₆₀O₅SSi

There total 15 articles about C₄₆H₆₀O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₅₆O₆Si

: 75-08-1
ethanethiol

: 1028432-63-4
C₄₆H₆₀O₅SSi

Guidance literature:: With zinc trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol800685c

Reference yield:

: 908865-92-9
(2S,3S)-6-(tert-Butyl-diphenyl-silanyloxy)-3-(4-methoxy-benzyloxy)-2-methyl-hexan-1-ol

: 1028432-63-4
C₄₆H₆₀O₅SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.75 h / 20 °C

2.1: tert.-butyl lithium; 9-methoxy-9-BBN / tetrahydrofuran; diethyl ether; hexane; pentane / 1.17 h / -78 - 20 °C

2.2: 50 °C

3.1: 2,3-Dimethyl-2-butene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

3.2: 0 - 20 °C

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / pH 7 / aq. phosphate buffer

6.1: zinc trifluoromethanesulfonate / dichloromethane / 12 h / 20 °C

With 1H-imidazole; tetrapropylammonium perruthennate; 2,3-Dimethyl-2-butene; dimethylsulfide borane complex; iodine; tert.-butyl lithium; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; 9-methoxy-9-BBN; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; pentane; 2.2: Suzuki-Miyaura coupling;
DOI:10.1002/chem.201101437

Reference yield:

: 1028432-61-2
C₅₂H₆₄O₆Si

: 1028432-63-4
C₄₆H₆₀O₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,3-Dimethyl-2-butene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / pH 7 / aq. phosphate buffer

4.1: zinc trifluoromethanesulfonate / dichloromethane / 12 h / 20 °C

With tetrapropylammonium perruthennate; 2,3-Dimethyl-2-butene; dimethylsulfide borane complex; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201101437