chloro-[2-(4-fluoro-phenyl)-3,4,5-trimethyl-cyclopenta-2,4-dienyl]-dimethyl-silane

Base Information

Chemical Name:chloro-[2-(4-fluoro-phenyl)-3,4,5-trimethyl-cyclopenta-2,4-dienyl]-dimethyl-silane
CAS No.:352712-03-9
Molecular Formula:C₁₆H₂₀ClFSi
Molecular Weight:294.872
Hs Code.:

Synonyms:chloro-[2-(4-fluoro-phenyl)-3,4,5-trimethyl-cyclopenta-2,4-dienyl]-dimethyl-silane

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Chemical Property of chloro-[2-(4-fluoro-phenyl)-3,4,5-trimethyl-cyclopenta-2,4-dienyl]-dimethyl-silane

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Technology Process of chloro-[2-(4-fluoro-phenyl)-3,4,5-trimethyl-cyclopenta-2,4-dienyl]-dimethyl-silane

There total 4 articles about chloro-[2-(4-fluoro-phenyl)-3,4,5-trimethyl-cyclopenta-2,4-dienyl]-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 1-(4-Fluorophenyl)-2,3,4-trimethylcyclopentadiene

: 352712-03-9
chloro-[2-(4-fluoro-phenyl)-3,4,5-trimethyl-cyclopenta-2,4-dienyl]-dimethyl-silane

Guidance literature:: 1-(4-Fluorophenyl)-2,3,4-trimethylcyclopentadiene; With n-butyllithium; In tetrahydrofuran; at 20 ℃;

dimethylsilicon dichloride; In tetrahydrofuran; Heating;
DOI:10.1135/cccc20010605

Reference yield:

: 28790-86-5
2,3,4-trimethylcyclopent-2-en-1-one

: 352712-03-9
chloro-[2-(4-fluoro-phenyl)-3,4,5-trimethyl-cyclopenta-2,4-dienyl]-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine

2.1: BuLi / tetrahydrofuran / 20 °C

2.2: 77 percent / tetrahydrofuran / Heating

With n-butyllithium; iodine; In tetrahydrofuran;
DOI:10.1135/cccc20010605

Reference yield:

: 130387-74-5
4-fluorophenylmagnesium chloride

: 352712-03-9
chloro-[2-(4-fluoro-phenyl)-3,4,5-trimethyl-cyclopenta-2,4-dienyl]-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine

2.1: BuLi / tetrahydrofuran / 20 °C

2.2: 77 percent / tetrahydrofuran / Heating

With n-butyllithium; iodine; In tetrahydrofuran;
DOI:10.1135/cccc20010605