1,4-diiodo-2,5-bis{[3,4,5-tri(hexoxy)phenyl]methoxy}benzene

Base Information

• Chemical Name: 1,4-diiodo-2,5-bis{[3,4,5-tri(hexoxy)phenyl]methoxy}benzene
• CAS No.: 217489-40-2
• Molecular Formula: C₅₆H₈₈I₂O₈
• Molecular Weight: 1143.12
• Mol file: 217489-40-2.mol

Synonyms:1,4-diiodo-2,5-bis{[3,4,5-tri(hexoxy)phenyl]methoxy}benzene

Chemical Property of 1,4-diiodo-2,5-bis{[3,4,5-tri(hexoxy)phenyl]methoxy}benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1,4-diiodo-2,5-bis{[3,4,5-tri(hexoxy)phenyl]methoxy}benzene

There total 1 articles about 1,4-diiodo-2,5-bis{[3,4,5-tri(hexoxy)phenyl]methoxy}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

3,4,5-tri-(hexoxy)benzyl chloride (420820-74-2) + 2,5-diiodo-1,4-hydroquinone (13064-64-7) → 1,4-diiodo-2,5-bis{[3,4,5-tri(hexoxy)phenyl]methoxy}benzene (217489-40-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c3ob00041a

Reference yield: 53.0%

4-pyridylacetylene (2510-22-7) + 1,4-diiodo-2,5-bis{[3,4,5-tri(hexoxy)phenyl]methoxy}benzene (217489-40-2) → 1,4-bis((4-pyridyl)ethynyl)-2,5-bis{[3,4,5-tri(butoxy)phenyl]methoxy}benzene (1443055-07-9)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; at 20 ℃; for 6h;

DOI:10.1039/c3ob00041a

upstream raw materials:

3,4,5-tri-(hexoxy)benzyl chloride

2,5-diiodo-1,4-hydroquinone

Downstream raw materials:

1,4-bis((4-pyridyl)ethynyl)-2,5-bis{[3,4,5-tri(butoxy)phenyl]methoxy}benzene