cis-4-phthaloylaminocyclohexanecarboxylic acid tert-butyl hydroperoxide ester

Base Information

Chemical Name:cis-4-phthaloylaminocyclohexanecarboxylic acid tert-butyl hydroperoxide ester
CAS No.:373391-77-6
Molecular Formula:C₁₉H₂₃NO₅
Molecular Weight:345.395
Hs Code.:

Synonyms:cis-4-phthaloylaminocyclohexanecarboxylic acid tert-butyl hydroperoxide ester

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Chemical Property of cis-4-phthaloylaminocyclohexanecarboxylic acid tert-butyl hydroperoxide ester

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Technology Process of cis-4-phthaloylaminocyclohexanecarboxylic acid tert-butyl hydroperoxide ester

There total 3 articles about cis-4-phthaloylaminocyclohexanecarboxylic acid tert-butyl hydroperoxide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 75-91-2
tert.-butylhydroperoxide

: 74196-46-6
N-phthaloyl-cis-4-aminocaclohexanecarboxylic acid

: 373391-77-6
cis-4-phthaloylaminocyclohexanecarboxylic acid tert-butyl hydroperoxide ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In decane; dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ja010799u

Reference yield:

: 85-44-9
phthalic anhydride

: 373391-77-6
cis-4-phthaloylaminocyclohexanecarboxylic acid tert-butyl hydroperoxide ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 0.25 h / 190 °C

2: 79 percent / DMAP; EDC*HCl / CH₂Cl₂; decane / 4 h / 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In decane; dichloromethane;
DOI:10.1021/ja010799u

Reference yield:

: 3685-23-2
cis-4-aminocyclohexane-1-carboxylic acid

: 373391-77-6
cis-4-phthaloylaminocyclohexanecarboxylic acid tert-butyl hydroperoxide ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 0.25 h / 190 °C

2: 79 percent / DMAP; EDC*HCl / CH₂Cl₂; decane / 4 h / 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In decane; dichloromethane;
DOI:10.1021/ja010799u