7-(3,5-Di-tert-butylphenyl)-2,12-bis(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Base Information

Chemical Name:7-(3,5-Di-tert-butylphenyl)-2,12-bis(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine
CAS No.:118656-26-1
Molecular Formula:C₆₅H₅₉N₃O₄
Molecular Weight:946.201
Hs Code.:

7-(3,5-Di-tert-butylphenyl)-2,12-bis(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenz<c,h>acridine

Synonyms:7-(3,5-Di-tert-butylphenyl)-2,12-bis(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

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Chemical Property of 7-(3,5-Di-tert-butylphenyl)-2,12-bis(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

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Technology Process of 7-(3,5-Di-tert-butylphenyl)-2,12-bis(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

There total 7 articles about 7-(3,5-Di-tert-butylphenyl)-2,12-bis(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32281-97-3
7-bromo-3,4-dihydro-2H-naphthalen-1-one

: 118656-26-1
7-(3,5-Di-tert-butylphenyl)-2,12-bis(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / p-toluenesulfonic acid / toluene / 12 h / Heating

3: 60 percent / 4percent KOH / methanol / 2.75 h / 75 °C

4: 1.) 70percent perchloric acid / 1.) 70 deg C, 4 h, 2.) C₂H₅OH

5: NH₃ / methanol; CH₂Cl₂ / 3 h / Ambient temperature

With potassium hydroxide; perchloric acid; ammonia; toluene-4-sulfonic acid; In methanol; dichloromethane; toluene;
DOI:10.1021/ja00186a035

Reference yield:

: 111773-13-8
7-Bromo-1,2,3,4-tetrahydronaphthalene-1-spiro-2'-(1',3'-dioxacyclopentane)

: 118656-26-1
7-(3,5-Di-tert-butylphenyl)-2,12-bis(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Guidance literature:: Multi-step reaction with 4 steps

2: 60 percent / 4percent KOH / methanol / 2.75 h / 75 °C

3: 1.) 70percent perchloric acid / 1.) 70 deg C, 4 h, 2.) C₂H₅OH

4: NH₃ / methanol; CH₂Cl₂ / 3 h / Ambient temperature

With potassium hydroxide; perchloric acid; ammonia; In methanol; dichloromethane;
DOI:10.1021/ja00186a035

Reference yield:

: 118656-09-0
7-(2,5-Dimethoxyacridin-9-yl)-1-oxo-1,2,3,4-tetrahydronaphthalene

: 118656-26-1
7-(3,5-Di-tert-butylphenyl)-2,12-bis(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / 4percent KOH / methanol / 2.75 h / 75 °C

2: 1.) 70percent perchloric acid / 1.) 70 deg C, 4 h, 2.) C₂H₅OH

3: NH₃ / methanol; CH₂Cl₂ / 3 h / Ambient temperature

With potassium hydroxide; perchloric acid; ammonia; In methanol; dichloromethane;
DOI:10.1021/ja00186a035