1,3,4,9a-tetrahydro-2-oxo-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12(2H)-dicarboxamide

Base Information

• Chemical Name: 1,3,4,9a-tetrahydro-2-oxo-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12(2H)-dicarboxamide
• CAS No.: 79234-19-8
• Molecular Formula: C₃₀H₂₈N₄O₃
• Molecular Weight: 492.577

Synonyms:1,3,4,9a-tetrahydro-2-oxo-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12(2H)-dicarboxamide

Chemical Property of 1,3,4,9a-tetrahydro-2-oxo-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12(2H)-dicarboxamide

Chemical Property:

Purity/Quality:

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Technology Process of 1,3,4,9a-tetrahydro-2-oxo-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12(2H)-dicarboxamide

There total 2 articles about 1,3,4,9a-tetrahydro-2-oxo-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12(2H)-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-<<2-(1H-indol-3-yl)ethyl>imino>cyclohexanone (79234-11-0) → 1,3,4,9a-tetrahydro-2-oxo-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12(2H)-dicarboxamide (79234-19-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 54 percent / conc. H₂SO₄ / 0.75 h / 100 °C

2: 1.8 g / tetrahydrofuran / 25 °C

With sulfuric acid; In tetrahydrofuran;

DOI:10.1021/jo00337a021

Reference yield:

phenyl isocyanate (103-71-9) + 3,4,9,9a-tetrahydro-1,4-ethano-3,4a-(iminoethano)-4aH-carbazol-2(1H)-one (79234-12-1) → 1,3,4,9a-tetrahydro-2-oxo-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12(2H)-dicarboxamide (79234-19-8)

Guidance literature:

In tetrahydrofuran; at 25 ℃;

DOI:10.1021/jo00337a021

Reference yield: 90.0%

1,3,4,9a-tetrahydro-2-oxo-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12(2H)-dicarboxamide (79234-19-8) → 1,3,4,9a-tetrahydro-2-hydroxy-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12-(2H)-dicarboxamide (79234-26-7)

Guidance literature:

With potassium borohydride; In methanol; at 23 ℃;

DOI:10.1021/jo00337a021

upstream raw materials:

phenyl isocyanate

3,4,9,9a-tetrahydro-1,4-ethano-3,4a-(iminoethano)-4aH-carbazol-2(1H)-one

2-<<2-(1H-indol-3-yl)ethyl>imino>cyclohexanone

Downstream raw materials:

3,3a,4,4a,10,10a-hexahydro-3a-hydroxy-2-oxo-N,3-diphenyl-1,9b:4,10-diethanoimidazo<4,5-b>carbazole-5(2H)-carboxamide

1,3,4,9a-tetrahydro-2-hydroxy-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12-(2H)-dicarboxamide

1,3,4,9a-tetrahydro-2-oxo-N,N'-diphenyl-1,4-ethano-3,4a-(iminoethano)-4aH-carbazole-9,12(2H)-dicarboxamide oxime

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