C₄₆H₄₇N₃O₇S₂Si

Base Information

Chemical Name:C₄₆H₄₇N₃O₇S₂Si
CAS No.:1057692-36-0
Molecular Formula:C₄₆H₄₇N₃O₇S₂Si
Molecular Weight:846.113
Hs Code.:

C<sub>46</sub>H<sub>47</sub>N<sub>3</sub>O<sub>7</sub>S<sub>2</sub>Si

Synonyms:C₄₆H₄₇N₃O₇S₂Si

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₆H₄₇N₃O₇S₂Si

Chemical Property:

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Technology Process of C₄₆H₄₇N₃O₇S₂Si

There total 1 articles about C₄₆H₄₇N₃O₇S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1057692-35-9
C₄₉H₅₁N₃O₇S₂Si

: 1057692-36-0
C₄₆H₄₇N₃O₇S₂Si

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja8046188

Reference yield:

: Fmoc-Gly-Wang resin

: 1057692-36-0
C₄₆H₄₇N₃O₇S₂Si

: 29022-11-5
N-(fluoren-9-ylmethoxycarbonyl)glycine

: 68858-20-8
Fmoc-Val-OH

: 35661-60-0
Fmoc-Leu-OH

: 71989-31-6
Fmoc-Pro-OH

: 108-24-7
acetic anhydride

: 71989-35-0,138797-71-4
Fmoc-Thr(tBu)-OH

: 100-53-8
phenylmethanethiol

: 187618-60-6
Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine

: 1190950-22-1
C₆₇H₁₀₁N₁₉O₁₆S₃

Guidance literature:: Fmoc-Gly-Wang resin; With 4-methylpiperidin; In N,N-dimethyl-formamide; for 0.25h; solid phase reaction;

Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; solid phase reaction;

C₄₆H₄₇N₃O₇S₂Si; N-(fluoren-9-ylmethoxycarbonyl)glycine; Fmoc-Val-OH; Fmoc-Leu-OH; Fmoc-Pro-OH; acetic anhydride; Fmoc-Thr(tBu)-OH; phenylmethanethiol; Further stages;
DOI:10.1002/anie.200902374

Reference yield:

: Fmoc-Gly-Wang resin

: 1057692-36-0
C₄₆H₄₇N₃O₇S₂Si

: 29022-11-5
N-(fluoren-9-ylmethoxycarbonyl)glycine

: 68858-20-8
Fmoc-Val-OH

: 35661-60-0
Fmoc-Leu-OH

: 71989-31-6
Fmoc-Pro-OH

: 108-24-7
acetic anhydride

: 100-53-8
phenylmethanethiol

: 175291-56-2
Fmoc-L-Thr(HPO₃Bzl)-OH

: 187618-60-6
Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine

: 1190950-23-2
C₆₇H₁₀₂N₁₉O₁₉PS₃

Guidance literature:: Fmoc-Gly-Wang resin; With 4-methylpiperidin; In N,N-dimethyl-formamide; for 0.25h; solid phase reaction;

Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; solid phase reaction;

C₄₆H₄₇N₃O₇S₂Si; N-(fluoren-9-ylmethoxycarbonyl)glycine; Fmoc-Val-OH; Fmoc-Leu-OH; Fmoc-Pro-OH; acetic anhydride; phenylmethanethiol; Fmoc-L-Thr(HPO₃Bzl)-OH; Further stages;
DOI:10.1002/anie.200902374