3β-hydroxy-16ξ-phenylsulfinyl-5-androsten-17-one 3-tetrahydropyranyl ether

Base Information

Chemical Name:3β-hydroxy-16ξ-phenylsulfinyl-5-androsten-17-one 3-tetrahydropyranyl ether
CAS No.:111119-48-3
Molecular Formula:C₃₀H₄₀O₄S
Molecular Weight:496.711
Hs Code.:

Synonyms:3β-hydroxy-16ξ-phenylsulfinyl-5-androsten-17-one 3-tetrahydropyranyl ether

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Chemical Property of 3β-hydroxy-16ξ-phenylsulfinyl-5-androsten-17-one 3-tetrahydropyranyl ether

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Technology Process of 3β-hydroxy-16ξ-phenylsulfinyl-5-androsten-17-one 3-tetrahydropyranyl ether

There total 1 articles about 3β-hydroxy-16ξ-phenylsulfinyl-5-androsten-17-one 3-tetrahydropyranyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 670-98-4
methyl benzenesulfinate

: 19637-35-5
3-tetrahydropyran-2-yloxy-androst-5-en-17-one

: 111119-48-3
3β-hydroxy-16ξ-phenylsulfinyl-5-androsten-17-one 3-tetrahydropyranyl ether

Guidance literature:: With sodium hydride; In diethyl ether; for 4h; Ambient temperature;

Reference yield: 87.0%

: 111119-48-3
3β-hydroxy-16ξ-phenylsulfinyl-5-androsten-17-one 3-tetrahydropyranyl ether

: 111119-50-7
3β-hydroxy-16ξ-phenylsulfinyl-5β-androsten-17-one

Guidance literature:: With toluene-4-sulfonic acid; In methanol; for 16h;

Reference yield:

: 111119-48-3
3β-hydroxy-16ξ-phenylsulfinyl-5-androsten-17-one 3-tetrahydropyranyl ether

: 17921-63-0
3β-hydroxy-androst-5,15-dien-17-one

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / aq. p-toluenesulfonic acid / methanol / 16 h

2: 57 percent / N,N-dimethylaniline / xylene / 15 h / Heating

With toluene-4-sulfonic acid; N,N-dimethyl-aniline; In methanol; xylene;