4-methoxy-o-phenyl phenyl(phenyl)phosphinate

Base Information

Chemical Name:4-methoxy-o-phenyl phenyl(phenyl)phosphinate
CAS No.:34253-15-1
Molecular Formula:C₁₉H₁₇O₃P
Molecular Weight:324.316
Hs Code.:

Synonyms:4-methoxy-o-phenyl phenyl(phenyl)phosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxy-o-phenyl phenyl(phenyl)phosphinate

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Technology Process of 4-methoxy-o-phenyl phenyl(phenyl)phosphinate

There total 12 articles about 4-methoxy-o-phenyl phenyl(phenyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 150-76-5
4-methoxy-phenol

: 4559-70-0
Diphenylphosphine oxide

: 34253-15-1
4-methoxy-o-phenyl phenyl(phenyl)phosphinate

Guidance literature:: With chloroform; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 25 ℃; for 3h;
DOI:10.1039/c9cc09407e

Reference yield: 99.0%

: 150-76-5
4-methoxy-phenol

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 34253-15-1
4-methoxy-o-phenyl phenyl(phenyl)phosphinate

Guidance literature:: 4-methoxy-phenol; chloro-diphenylphosphine; With triethylamine; In dichloromethane; at 20 ℃; for 12h;

With dihydrogen peroxide; Further stages.;
DOI:10.1016/j.tetlet.2004.03.073

Reference yield: 94.0%

: 1054-59-7
1,1,2,2-tetraphenyldiphosphane-1,2-dioxide

: 150-76-5
4-methoxy-phenol

: 34253-15-1
4-methoxy-o-phenyl phenyl(phenyl)phosphinate

Guidance literature:: With hydridotetakis(triphenylphosphine)rhodium(I); 1,2-bis(dimethylphosphanyl)ethane; In tetrahydrofuran; for 3h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2010.07.040