5-((2E)-3,7-dimethyl-2,6-octadien-1-yl)-3,4-bis(methoxymethoxy)benzyloxy(tert-butyl)dimethylsilane

Base Information

Chemical Name:5-((2E)-3,7-dimethyl-2,6-octadien-1-yl)-3,4-bis(methoxymethoxy)benzyloxy(tert-butyl)dimethylsilane
CAS No.:1069118-51-9
Molecular Formula:C₂₇H₄₆O₅Si
Molecular Weight:478.745
Hs Code.:

Synonyms:5-((2E)-3,7-dimethyl-2,6-octadien-1-yl)-3,4-bis(methoxymethoxy)benzyloxy(tert-butyl)dimethylsilane

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Chemical Property of 5-((2E)-3,7-dimethyl-2,6-octadien-1-yl)-3,4-bis(methoxymethoxy)benzyloxy(tert-butyl)dimethylsilane

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Technology Process of 5-((2E)-3,7-dimethyl-2,6-octadien-1-yl)-3,4-bis(methoxymethoxy)benzyloxy(tert-butyl)dimethylsilane

There total 1 articles about 5-((2E)-3,7-dimethyl-2,6-octadien-1-yl)-3,4-bis(methoxymethoxy)benzyloxy(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6138-90-5
trans-geranyl bromide

: 1069118-50-8
{[3-bromo-4,5-bis(methoxymethoxy)benzyl]oxy}(tert-butyl)dimethylsilane

: 1069118-51-9
5-((2E)-3,7-dimethyl-2,6-octadien-1-yl)-3,4-bis(methoxymethoxy)benzyloxy(tert-butyl)dimethylsilane

Guidance literature:: {[3-bromo-4,5-bis(methoxymethoxy)benzyl]oxy}(tert-butyl)dimethylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

trans-geranyl bromide; In tetrahydrofuran; hexane; at 20 ℃; for 16h; Further stages.;
DOI:10.1021/jo800951q

Reference yield:

: 1069118-51-9
5-((2E)-3,7-dimethyl-2,6-octadien-1-yl)-3,4-bis(methoxymethoxy)benzyloxy(tert-butyl)dimethylsilane

: 5-((2E)-3,7-dimethyl-6-epoxyoct-2-en-1-yl)-3,4-bis(methoxymethoxy)benzyloxy(tert-butyl)dimethylsilane

: 1069118-52-0
5-((2E)-3,7-dimethyl-6-epoxyoct-2-en-1-yl)-3,4-bis(methoxymethoxy)benzyloxy(tert-butyl)dimethylsilane

Guidance literature:: With ethylenediaminetetraacetic acid; dihydrogen peroxide; potassium carbonate; In acetonitrile; butan-1-ol; for 22h; Title compound not separated from byproducts.; cooling;
DOI:10.1021/jo800951q