16-(N-Boc-S-trityl-cysteinylamido)hexadecanoic acid

Base Information

Chemical Name:16-(N-Boc-S-trityl-cysteinylamido)hexadecanoic acid
CAS No.:1296794-75-6
Molecular Formula:C₄₃H₆₀N₂O₅S
Molecular Weight:717.026
Hs Code.:

Synonyms:16-(N-Boc-S-trityl-cysteinylamido)hexadecanoic acid

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Chemical Property of 16-(N-Boc-S-trityl-cysteinylamido)hexadecanoic acid

Chemical Property:

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Technology Process of 16-(N-Boc-S-trityl-cysteinylamido)hexadecanoic acid

There total 5 articles about 16-(N-Boc-S-trityl-cysteinylamido)hexadecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1296794-74-5
ethyl 16-(N-Boc-S-trityl-cysteinylamido)hexadecanoate

: 1296794-75-6
16-(N-Boc-S-trityl-cysteinylamido)hexadecanoic acid

Guidance literature:: ethyl 16-(N-Boc-S-trityl-cysteinylamido)hexadecanoate; With potassium hydroxide; In methanol; water; at 20 ℃; for 48h;

With hydrogenchloride; In water; pH=3;
DOI:10.1002/jlcr.1836

Reference yield:

: 110504-18-2
C₁₆H₃₃NO₂*ClH

: 1296794-75-6
16-(N-Boc-S-trityl-cysteinylamido)hexadecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / Reflux

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

3.1: potassium hydroxide / methanol; water / 48 h / 20 °C

3.2: pH 3

With sulfuric acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In methanol; dichloromethane; water;
DOI:10.1002/jlcr.1836

Reference yield:

: ethyl 16-phthalimidohexadecanoate

: 1296794-75-6
16-(N-Boc-S-trityl-cysteinylamido)hexadecanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / ethanol / 3 h / Reflux

1.2: Reflux

2.1: sulfuric acid / Reflux

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

4.1: potassium hydroxide / methanol; water / 48 h / 20 °C

4.2: pH 3

With sulfuric acid; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In methanol; ethanol; dichloromethane; water;
DOI:10.1002/jlcr.1836