Technology Process of C44H51F2N13O15
There total 3 articles about C44H51F2N13O15 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine; isobutyl chloroformate;
In
N,N-dimethyl-formamide;
at -10 ℃;
for 8h;
Inert atmosphere;
DOI:10.2174/15701786113109990024
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.42 h / 0 °C / Inert atmosphere
1.2: 24 h / 20 °C / Inert atmosphere
2.1: palladium 10% on activated carbon; hydrogen / methanol / 12 h / 20 °C / Inert atmosphere
3.1: 4-methyl-morpholine; isobutyl chloroformate / N,N-dimethyl-formamide / 8 h / -10 °C / Inert atmosphere
With
4-methyl-morpholine; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; isobutyl chloroformate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.2174/15701786113109990024
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 12 h / 20 °C / Inert atmosphere
2: 4-methyl-morpholine; isobutyl chloroformate / N,N-dimethyl-formamide / 8 h / -10 °C / Inert atmosphere
With
4-methyl-morpholine; palladium 10% on activated carbon; hydrogen; isobutyl chloroformate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.2174/15701786113109990024