7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid sodium salt

Base Information

Chemical Name:7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid sodium salt
CAS No.:1447673-36-0
Molecular Formula:C₂₈H₃₂N₃O₂*Na
Molecular Weight:465.571
Hs Code.:

Synonyms:7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid sodium salt

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Chemical Property of 7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid sodium salt

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Technology Process of 7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid sodium salt

There total 7 articles about 7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356331-63-9
7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid

: 1447673-36-0
7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid sodium salt

Guidance literature:: With sodium hydroxide; In water; at 20 ℃; Solvent; Temperature;

Reference yield:

: 3990-05-4
ethyl 6-formylhexanoate

: 1447673-36-0
7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid sodium salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 0.17 h / 20 °C

1.2: 20 - 40 °C

2.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 7.5 h / 50 °C

3.1: sodium hydroxide / water / 20 °C

With lithium hydroxide monohydrate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; water; 1,2-dichloro-ethane;

Reference yield:

: 2,3-di-p-tolylpyrido[2,3-b]pyrazine acetate

: 1447673-36-0
7-(2,3-di-p-tolyl-7,8-dihydropyrido[2,3-b]pyrazin-5(6H)-yl)heptanoic acid sodium salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium 10% on activated carbon; hydrogen; triethylamine / tetrahydrofuran; ethanol / 168 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 0.17 h / 20 °C

2.2: 20 - 40 °C

3.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 7.5 h / 50 °C

4.1: sodium hydroxide / water / 20 °C

With lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; ethanol; water; 1,2-dichloro-ethane;