C₃₂H₄₂F₂N₆O₆Si

Base Information

Chemical Name:C₃₂H₄₂F₂N₆O₆Si
CAS No.:1202760-75-5
Molecular Formula:C₃₂H₄₂F₂N₆O₆Si
Molecular Weight:672.804
Hs Code.:

C<sub>32</sub>H<sub>42</sub>F<sub>2</sub>N<sub>6</sub>O<sub>6</sub>Si

Synonyms:C₃₂H₄₂F₂N₆O₆Si

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Chemical Property of C₃₂H₄₂F₂N₆O₆Si

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Technology Process of C₃₂H₄₂F₂N₆O₆Si

There total 10 articles about C₃₂H₄₂F₂N₆O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.8%

: 575474-26-9
2-chloro-N₄-(3-nitrophenyl)-5-fluoro-4-pyrimidineamine

: 1202760-86-8
C₂₂H₃₇FN₂O₄Si

: 1202760-75-5
C₃₂H₄₂F₂N₆O₆Si

Guidance literature:: With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; In toluene; at 110 ℃; for 16h; Inert atmosphere;

Reference yield:

: 40216-83-9
L-4-hydroxyproline methyl ester hydrochloride

: 1202760-75-5
C₃₂H₄₂F₂N₆O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane / 5 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 16 h

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / -20 °C

4: di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5: hydrogen / palladium on activated carbon / methanol / 16 h / 20 °C

6: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 16 h / 110 °C / Inert atmosphere

With 1H-imidazole; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; hydrogen; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; triphenylphosphine; palladium on activated carbon; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1202760-75-5
C₃₂H₄₂F₂N₆O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane / 5 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 16 h

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / -20 °C

4: di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5: hydrogen / palladium on activated carbon / methanol / 16 h / 20 °C

6: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 16 h / 110 °C / Inert atmosphere

With 1H-imidazole; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; hydrogen; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; triphenylphosphine; palladium on activated carbon; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;